ChemicalBook > CAS DataBase List > Ethanone, 1-(4-pyridazinyl)- (9CI)

Ethanone, 1-(4-pyridazinyl)- (9CI)

Product Name: Ethanone, 1-(4-pyridazinyl)- (9CI)
CAS No.: 50901-46-7
Chemical Name: Ethanone, 1-(4-pyridazinyl)- (9CI)
Synonyms: 4-Acetylpyridazine;1-(Pyridazin-4-yl);4-Acetylpyridazine,95%;1-(4-Pyridazinyl)ethanone;1-(Pyridazin-4-yl)ethanone;Methyl 4-pyridazinyl ketone;Ethanone, 1-(4-pyridazinyl)-;1-(pyridazin-4-yl)ethan-1-one;Ethanone, 1-(4-pyridazinyl)- (9CI);1-(PYRIDAZIN-4-YL)ETHANONE，1-(PYRIDAZIN-4-YL)ETHAN-1-ONE
CBNumber: CB11063920
Molecular Formula: C6H6N2O
Formula Weight: 122.12
MOL File: 50901-46-7.mol

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Ethanone, 1-(4-pyridazinyl)- (9CI) Property

Melting point:: 69-70℃
Boiling point:: 285.9±13.0 °C(Predicted)
Density: 1.136±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Sealed in dry,Store in freezer, under -20°C
pka: 0.50±0.10(Predicted)
form: Solid
Appearance: Light brown to brown Solid
InChI: InChI=1S/C6H6N2O/c1-5(9)6-2-3-7-8-4-6/h2-4H,1H3
InChIKey: IWFYWGOLMZIBQB-UHFFFAOYSA-N
SMILES: C(=O)(C1=CC=NN=C1)C
CAS DataBase Reference: 50901-46-7

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: P993400
Product name: 1-(Pyridazin-4-yl)ethanone
Packaging: 500mg
Price: $265
Updated: 2021/12/16

Matrix Scientific

Product number: 119000
Product name: 1-(Pyridazin-4-yl)ethanone
Purity: 95+%
Packaging: 250mg
Price: $339
Updated: 2021/12/16

Matrix Scientific

Product number: 119000
Product name: 1-(Pyridazin-4-yl)ethanone
Purity: 95+%
Packaging: 1g
Price: $846
Updated: 2021/12/16

AK Scientific

Product number: W6606
Product name: 1-(Pyridazin-4-yl)ethanone
Packaging: 5g
Price: $1061
Updated: 2021/12/16

Ambeed

Product number: A388934
Product name: 1-(Pyridazin-4-yl)ethanone
Purity: 98%
Packaging: 250mg
Price: $87
Updated: 2021/12/16

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Ethanone, 1-(4-pyridazinyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

823189-69-1

75-16-1

50901-46-7

GENERAL STEPS: Methylmagnesium bromide (10.1 mL, 10.1 mmol, 1 M solution in ether) was added slowly and dropwise to a solution of N-methoxy-N-methylpyridazine-4-carboxamide (1.13 g, 6.76 mmol) in tetrahydrofuran (22 mL) under nitrogen protection. The reaction mixture was stirred at room temperature for 1 hour. Upon completion of the reaction, the reaction solution was mixed with saturated aqueous sodium chloride solution and extracted with chloroform. The organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate=1/2→0/1) to afford 1-(pyridazin-4-yl)ethanone in 42% yield. Product characterization: light yellow solid; LC/MS (condition 7): retention time 0.75 min; LC/MS (ESI+) m/z: 123 [M+H]+; 1H-NMR (CDCl3) δ: 2.70 (s, 3H), 7.86 (dd, J=0.8 and 5.4 Hz, 1H), 9.48 (d, J=5.4 Hz, 1H),. 9.61 (d, J=0.8 Hz, 1H).

References

[1] Patent: WO2009/57827, 2009, A1. Location in patent: Page/Page column 127-128

Ethanone, 1-(4-pyridazinyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethanone, 1-(4-pyridazinyl)- (9CI) manufacturers

Nanjing jinheyou Trading Co., Ltd.

Product: 1-Pyridazin-4-yl-ethanone 50901-46-7
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 20kgs/month
Release date: 2019-11-13

50901-46-7, Ethanone, 1-(4-pyridazinyl)- (9CI)Related Search:

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Ethanone, 1-(4-pyridazinyl)-

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1-(Pyridazin-4-yl)

Ethanone, 1-(4-pyridazinyl)- (9CI)

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4-Acetylpyridazine,95%

1-(4-Pyridazinyl)ethanone

50901-46-7

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