ChemicalBook > CAS DataBase List > 4-AMINO-2,3-XYLENOL

4-AMINO-2,3-XYLENOL

Product Name
4-AMINO-2,3-XYLENOL
CAS No.
3096-69-3
Chemical Name
4-AMINO-2,3-XYLENOL
Synonyms
4-AMINO-2,3-XYLENOL;4-Amino-2,3-xylenol >4-AMINO-2,3-XYLENOL 97+%;4-amino-2,3-dimethylphenol;2,3-DIMETHYL-4-AMINOPHENOL;4-azanyl-2,3-dimethyl-phenol;4-hydroxy-2,3-dimethylaniline;2,3-Dimethyl-4-hydroxyaniline;Phenol, 4-amino-2,3-dimethyl-;4-Amino-2,3-dimethylphenol 4-Hydroxy-2,3-dimethylaniline
CBNumber
CB1114007
Molecular Formula
C8H11NO
Formula Weight
137.18
MOL File
3096-69-3.mol
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4-AMINO-2,3-XYLENOL Property

Melting point:
174°C
Boiling point:
296.3±28.0 °C(Predicted)
Density 
1.118±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
10.70±0.23(Predicted)
color 
White to Gray to Brown
CAS DataBase Reference
3096-69-3
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Safety

Risk Statements 
20/21/22-36/37/38
Safety Statements 
26-36/37/39
HS Code 
2922.29.8190
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
A0961
Product name
4-Amino-2,3-xylenol
Purity
>98.0%(GC)(T)
Packaging
10g
Price
$302
Updated
2025/07/31
TRC
Product number
A597150
Product name
4-Amino-2,3-dimethylphenol
Packaging
500mg
Price
$110
Updated
2021/12/16
Matrix Scientific
Product number
119634
Product name
4-Amino-2,3-dimethylphenol
Purity
95+%
Packaging
1g
Price
$180
Updated
2021/12/16
Matrix Scientific
Product number
119634
Product name
4-Amino-2,3-dimethylphenol
Purity
95+%
Packaging
5g
Price
$540
Updated
2021/12/16
AK Scientific
Product number
Y5379
Product name
4-Amino-2,3-dimethylphenol
Packaging
10g
Price
$563
Updated
2021/12/16
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4-AMINO-2,3-XYLENOL Chemical Properties,Usage,Production

Synthesis

19499-93-5

3096-69-3

General procedure for the synthesis of 4-amino-2,3-xylenol from 2,3-dimethyl-4-nitrophenol: A mixture of 2,3-dimethyl-4-nitrophenol (2 g, 1.2 mmol) with 10% Pd/C catalyst (1.83 g) in ethanol (80 mL) was placed under hydrogen atmosphere and reacted with stirring at room temperature for 5 hours. Upon completion of the reaction, the crude reaction mixture was filtered through diatomaceous earth and the filter cake was washed with dichloromethane (DCM). After evaporation to remove the solvent, 4-amino-2,3-xylenol (1.60 g, 97% yield) was obtained as a brown powder. The product was characterized by 1H-NMR (DMSO-d6): δ 1.94 (s, 3H, methyl proton), 2.01 (s, 3H, methyl proton), 4.06 (s, 2H, amino proton), 6.32 (d, 1H, aromatic proton H-6, J = 8.1 Hz), 6.40 (d, 1H, aromatic proton H-5, J = 8.1 Hz), 6.61 (s , 1H, aromatic proton H-2), 8.10 (broad s, 1H, hydroxyl proton).

References

[1] Patent: WO2006/43090, 2006, A1. Location in patent: Page/Page column 176
[2] Journal of Medicinal Chemistry, 2009, vol. 52, # 13, p. 3881 - 3891

4-AMINO-2,3-XYLENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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  • 4-AMINO-2,3-XYLENOL
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  • 1-chloro-2-[1-chloropropan-2-yloxy(1-methylethenyl)phosphoryl]oxypropane
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  • 2,3-Dimethyl-4-hydroxyaniline
  • 3096-69-3