2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE

Product Name: 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE
CAS No.: 34165-09-8
Chemical Name: 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE
Synonyms: 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE;Imidazo[1,2-a]pyridine, 2-methyl-3-nitro-;2-Methyl-3-nitroimidazo[1,2-a]pyridine[N/A]
CBNumber: CB11253455
Molecular Formula: C8H7N3O2
Formula Weight: 177.16
MOL File: 34165-09-8.mol

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2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE Property

storage temp.: 2-8°C
Appearance: Off-white to light yellow Solid

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M341893
Product name: 2-Methyl-3-nitroimidazo[1,2-a]pyridine
Packaging: 500mg
Price: $310
Updated: 2021/12/16

Matrix Scientific

Product number: 085990
Product name: 2-Methyl-3-nitroimidazo[1,2-a]pyridine
Purity: 97%
Packaging: 1g
Price: $323
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0069311
Product name: 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE
Purity: 95.00%
Packaging: 1G
Price: $776.16
Updated: 2021/12/16

AK Scientific

Product number: 4076AB
Product name: 2-Methyl-3-nitroimidazo[1,2-a]pyridine
Packaging: 1g
Price: $832
Updated: 2021/12/16

Ambeed

Product number: A475626
Product name: 2-Methyl-3-nitroimidazo[1,2-a]pyridine
Purity: 97%
Packaging: 5g
Price: $1476
Updated: 2021/12/16

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2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE Chemical Properties,Usage,Production

Synthesis

934-37-2

34165-09-8

General procedure for the synthesis of 2-methyl-3-nitroimidazo[1,2-a]pyridine from 2-methylimidazo[1,2-a]pyridine: to a cooled solution of 2-methylimidazo[1,2-a]pyridine (380 mg, 2.88 mmol) in concentrated sulfuric acid (6 mL) was slowly added nitric acid (472 μL, density = 1.38 g/mL) dropwise. The reaction mixture was stirred for 2 h at room temperature and then cooled in an ice bath, followed by slow addition of saturated aqueous Na2CO3 solution adjusted to alkaline. The reaction mixture was extracted with dichloromethane (CH2Cl2) and the organic layer was dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to give 330 mg (1.82 mmol, 65% yield) of 2-methyl-3-nitroimidazo[1,2-a]pyridine as a brown solid.LRMS (m/z): 178 ([M+H]+).

References

[1] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 22, p. 7155 - 7164
[2] Patent: EP2848615, 2015, A1. Location in patent: Paragraph 0099
[3] Chemical and Pharmaceutical Bulletin, 2001, vol. 49, # 12, p. 1631 - 1635

2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE Suppliers

China 22 India 2 United Kingdom 1 United States 1 Global 26

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34165-09-8, 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINERelated Search:

3-NITROIMIDAZO[1,2-A]PYRIDINE ETHYL 6-CHLORO-3-NITROIMIDAZO[1,2-A]PYRIDINE-2-CARBOXYLATE BUTTPARK 12\01-50 BUTTPARK 38\01-30 2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE (6-BROMO-3-NITROIMIDAZO[1,2-A]PYRIDIN-2-YL)METHANOL BUTTPARK 38\01-33 6-BROMO-2-CHLOROMETHYL-3-NITROIMIDAZO[1,2-A] PYRIDINE BUTTPARK 38\01-40 BUTTPARK 38\01-35

2-METHYL-3-NITROIMIDAZO[1,2-A]PYRIDINE

Imidazo[1,2-a]pyridine, 2-methyl-3-nitro-

2-Methyl-3-nitroimidazo[1,2-a]pyridine[N/A]

34165-09-8

Fused Ring Systems