3-Pyridinemethanamine,2-methoxy-(9CI)
- Product Name
- 3-Pyridinemethanamine,2-methoxy-(9CI)
- CAS No.
- 354824-19-4
- Chemical Name
- 3-Pyridinemethanamine,2-methoxy-(9CI)
- Synonyms
- 2-Methoxy-3-PyridineMethanaMine;3-AMinoMethyl-2-Methoxypyridine;(2-methoxy-3-pyridyl)methylamine;(2-methoxy-3-pyridyl)methanamine;3-PyridineMethanaMine, 2-Methoxy-;(2-METHOXYPYRIDIN-3-YL)METHANAMINE;(2-methoxy-3-pyridinyl)methanamine;C-(2-Methoxypyridin-3-yl)MethanaMine;3-Pyridinemethanamine,2-methoxy-(9CI);C-(2-Methoxy-pyridin-3-yl)-methylamine
- CBNumber
- CB11289294
- Molecular Formula
- C7H10N2O
- Formula Weight
- 138.17
- MOL File
- 354824-19-4.mol
3-Pyridinemethanamine,2-methoxy-(9CI) Property
- Boiling point:
- 224.7±25.0 °C(Predicted)
- Density
- 1.090±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 7.60±0.29(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- A613880
- Product name
- 3-Aminomethyl-2-methoxypyridine
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CS-W021066
- Product name
- (2-Methoxypyridin-3-yl)methanamine
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- CS-W021066
- Product name
- (2-Methoxypyridin-3-yl)methanamine
- Packaging
- 1g
- Price
- $114
- Updated
- 2021/12/16
- Product number
- 064230
- Product name
- [(2-Methoxypyridin-3-yl)methyl]amine
- Packaging
- 500mg
- Price
- $237
- Updated
- 2021/12/16
- Product number
- CS-W021066
- Product name
- (2-Methoxypyridin-3-yl)methanamine
- Packaging
- 5g
- Price
- $310
- Updated
- 2021/12/16
3-Pyridinemethanamine,2-methoxy-(9CI) Chemical Properties,Usage,Production
Synthesis
71255-09-9
354824-19-4
Example 11: Synthesis of 3-aminomethyl-2-methoxypyridine (25) To a round bottom flask was added 2-methoxy-3-pyridinecarboxaldehyde (24) (0.44 g, 3.23 mmol), ammonium acetate (1.24 g, 16.15 mmol) and sodium cyanoborohydride (0.61 g, 19.69 mmol). After replacing the atmosphere in the flask with argon, dry methanol (50 mL) was added via syringe. The reaction mixture was stirred for 2 days and subsequently concentrated under reduced pressure to remove the methanol. To the residue, water (25 mL) was added and the pH was adjusted to 2 with concentrated hydrochloric acid. two extractions with ethyl acetate were performed to remove the alcoholic by-products. Subsequently, the pH of the aqueous phase was adjusted to 10 with sodium hydroxide pellets, saturated with sodium chloride and extracted twice with dichloromethane and once with ethyl acetate. The organic phases were combined, dried and concentrated under reduced pressure to give 3-aminomethyl-2-methoxypyridine (25) (0.31 g, 69% yield).
References
[1] Patent: WO2006/108103, 2006, A1. Location in patent: Page/Page column 32
[2] Patent: US2008/119496, 2008, A1. Location in patent: Page/Page column 11
[3] Patent: WO2008/60301, 2008, A1. Location in patent: Page/Page column 31
3-Pyridinemethanamine,2-methoxy-(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Pyridinemethanamine,2-methoxy-(9CI) manufacturers
- Product
- 3-Pyridinemethanamine,2-methoxy-(9CI) 354824-19-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1lg; 2kg; 5kg; 10kg; 100kg
- Release date
- 2019-08-31