2-PHENYLETHYLMETHANESULPHONATE
- Product Name
- 2-PHENYLETHYLMETHANESULPHONATE
- CAS No.
- 20020-27-3
- Chemical Name
- 2-PHENYLETHYLMETHANESULPHONATE
- Synonyms
- 3-phenylpropane-1-sulfonate;2-PHENYLETHYLMETHANESULPHONATE;2-phenylethyl methanesulfonate;Methanesulfonic acid, 2-phenylethyl ester
- CBNumber
- CB11445065
- Molecular Formula
- C9H12O3S
- Formula Weight
- 200.25
- MOL File
- 20020-27-3.mol
2-PHENYLETHYLMETHANESULPHONATE Property
- Boiling point:
- 358.1±21.0 °C(Predicted)
- Density
- 1.205±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
N-Bromosuccinimide Price
- Product number
- 61-10142
- Product name
- Phenethylmethanesulfonate
- Purity
- 95-98%
- Packaging
- 1g
- Price
- $225
- Updated
- 2021/12/16
- Product number
- 20020273
- Product name
- Phenethylmethanesulfonate
- Packaging
- 5g
- Price
- $352.8
- Updated
- 2021/12/16
- Product number
- CD12098755
- Product name
- Phenethylmethanesulfonate
- Purity
- 98%
- Packaging
- 5g
- Price
- $356
- Updated
- 2021/12/16
- Product number
- CD12098755
- Product name
- Phenethylmethanesulfonate
- Purity
- 98%
- Packaging
- 10g
- Price
- $594
- Updated
- 2021/12/16
- Product number
- 20020273
- Product name
- Phenethylmethanesulfonate
- Packaging
- 10g
- Price
- $594
- Updated
- 2021/12/16
2-PHENYLETHYLMETHANESULPHONATE Chemical Properties,Usage,Production
Synthesis
60-12-8
124-63-0
20020-27-3
GENERAL METHOD: Phenylethanol (2.14 mmol) was dissolved in anhydrous dichloromethane (6 mL) with triethylamine (0.36 mL, 2.59 mmol) under nitrogen protection and cooled to 0 °C. Subsequently, methanesulfonyl chloride (0.18 mL, 2.31 mmol) was slowly added dropwise and the reaction temperature was maintained at 0 °C for 1 hour. After that, the reaction mixture was gradually warmed up to room temperature and stirring was continued for 3 hours. After completion of the reaction, the reaction mixture was extracted with dichloromethane (3 x 30 mL). The organic phases were combined and washed sequentially with 10% aqueous hydrochloric acid and saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure, and the resulting crude product was purified by silica gel column chromatography, sequentially using dichloromethane and chloroform as eluents, to obtain the target product, phenethyl methanesulfonate, the structure of which was confirmed by the method described in the Supplementary Material.
References
[1] European Journal of Medicinal Chemistry, 2011, vol. 46, # 7, p. 3000 - 3012
[2] Synthetic Communications, 2011, vol. 41, # 5, p. 748 - 753
[3] Journal of Organic Chemistry, 1993, vol. 58, # 1, p. 272 - 274
[4] Tetrahedron, 2016, vol. 72, # 49, p. 8022 - 8030
[5] Journal of Medicinal Chemistry, 1990, vol. 33, # 10, p. 2807 - 2813
2-PHENYLETHYLMETHANESULPHONATE Preparation Products And Raw materials
Raw materials
Preparation Products
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