ChemicalBook > CAS DataBase List > 5-propan-2-yl-1H-indole-2,3-dione

5-propan-2-yl-1H-indole-2,3-dione

Product Name
5-propan-2-yl-1H-indole-2,3-dione
CAS No.
150560-58-0
Chemical Name
5-propan-2-yl-1H-indole-2,3-dione
Synonyms
11J-308S;ZINC03276921;5-Isopropylisatin;5-Isopropylindoline-2,3-dione;5-propan-2-yl-1H-indole-2,3-dione;1H-Indole-2,3-dione, 5-isopropyl-;5,5-dimethylcyclohex an-1, 3-dion;1H-Indole-2,3-dione, 5-(1-methylethyl)-;5-isopropyl-1H-indole-2,3-dione(SALTDATA: FREE);organic chemicals : 5,5-dimethylcyclohex an-1, 3-dion
CBNumber
CB11454834
Molecular Formula
C11H11NO2
Formula Weight
189.21
MOL File
150560-58-0.mol
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5-propan-2-yl-1H-indole-2,3-dione Property

Melting point:
140 °C
Density 
1.200±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
9.81±0.20(Predicted)
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Safety

Risk Statements 
36
Safety Statements 
26
RIDADR 
UN 2811 6.1 / PGIII
HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
I873465
Product name
5-Isopropyl-1H-indole-2,3-dione
Packaging
500mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
156189
Product name
5-Isopropyl-1H-indole-2,3-dione
Packaging
0.500g
Price
$120
Updated
2021/12/16
Apolloscientific
Product number
OR951185
Product name
5-Isopropyl-1H-indole-2,3-dione
Purity
95%
Packaging
1g
Price
$130
Updated
2021/12/16
AK Scientific
Product number
V3444
Product name
5-Isopropyl-1h-indole-2,3-dione
Packaging
1g
Price
$157
Updated
2021/12/16
Apolloscientific
Product number
OR951185
Product name
5-Isopropyl-1H-indole-2,3-dione
Purity
95%
Packaging
5g
Price
$360
Updated
2021/12/16
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5-propan-2-yl-1H-indole-2,3-dione Chemical Properties,Usage,Production

Synthesis

68701-52-0

150560-58-0

The general procedure for the synthesis of 5-isopropylindoline-2,3-dione using the compound (CAS: 68701-52-0) as starting material was as follows: 41.2 g of isonitrosoacetyl-p-isopropylaniline was slowly added to 294 g of 95% sulfuric acid at room temperature. Subsequently, the temperature of the reaction system was gradually increased to 30°C over a period of 10 minutes and the reaction mixture was continuously stirred at this temperature for 2 hours. Upon completion of the reaction, the reaction solution was slowly added dropwise to a separate vessel containing 419 g of water and the precipitate precipitated was subsequently collected by filtration. The precipitate was washed with 1,300 g of water and dried in a drying oven at 60 °C to yield 37.3 g of 5-isopropylisatin. The yield of this step was 98.7%, the purity of the product was 98.1% (wt%) and the melting point was 137-140 °C. In this embodiment, the molar ratio of isonitrosoacetyl-p-isopropylaniline to sulfuric acid was 1:14.3.

References

[1] Patent: JP2018/150285, 2018, A. Location in patent: Paragraph 0024-0031; 0036
[2] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004, vol. 43, # 7, p. 1585 - 1587

5-propan-2-yl-1H-indole-2,3-dione Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-propan-2-yl-1H-indole-2,3-dione manufacturers

Wuhan KEMI-WORKS Chemical Co., Ltd.
Product
5-Isopropyl Isatin 150560-58-0
Price
US $0.00/kg
Min. Order
1kg
Purity
98.0% min
Supply Ability
10tons
Release date
2024-08-06
Honest Joy Holdings Limited
Product
5-Isopropyl-1h-indole-2,3-dione 150560-58-0
Price
US $0.00/KG
Min. Order
1KG
Purity
99.3%
Supply Ability
100 tons
Release date
2022-02-08

150560-58-0, 5-propan-2-yl-1H-indole-2,3-dioneRelated Search:


  • 5-propan-2-yl-1H-indole-2,3-dione
  • 5-Isopropylisatin
  • 5-Isopropylindoline-2,3-dione
  • 11J-308S
  • 1H-Indole-2,3-dione, 5-isopropyl-
  • ZINC03276921
  • 5-isopropyl-1H-indole-2,3-dione(SALTDATA: FREE)
  • organic chemicals : 5,5-dimethylcyclohex an-1, 3-dion
  • 5,5-dimethylcyclohex an-1, 3-dion
  • 1H-Indole-2,3-dione, 5-(1-methylethyl)-
  • 150560-58-0