N-ETHYL-N-(4-FLUOROPHENYL)AMINE
- Product Name
- N-ETHYL-N-(4-FLUOROPHENYL)AMINE
- CAS No.
- 405-67-4
- Chemical Name
- N-ETHYL-N-(4-FLUOROPHENYL)AMINE
- Synonyms
- 100156;ethyl(4-fluorophenyl)amine;N-Ethyl-4-fluoro-benzenaMine;BenzenaMine,N-ethyl-4-fluoro-
- CBNumber
- CB11489333
- Molecular Formula
- C8H10FN
- Formula Weight
- 139.17
- MOL File
- 405-67-4.mol
N-ETHYL-N-(4-FLUOROPHENYL)AMINE Property
- Boiling point:
- 92 °C(Press: 14 Torr)
- Density
- 1.073±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 5.22±0.32(Predicted)
Safety
- HazardClass
- IRRITANT
- HS Code
- 2921199990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H317May cause an allergic skin reaction
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
N-Bromosuccinimide Price
- Product number
- E939420
- Product name
- N-Ethyl-4-fluoroaniline
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- PC907920
- Product name
- N-ethyl-4-fluoroaniline
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 062566
- Product name
- N-Ethyl-4-fluoroaniline
- Packaging
- 500mg
- Price
- $163
- Updated
- 2021/12/16
- Product number
- 5502AB
- Product name
- N-Ethyl-4-fluoroaniline
- Packaging
- 1g
- Price
- $267
- Updated
- 2021/12/16
- Product number
- 062566
- Product name
- N-Ethyl-4-fluoroaniline
- Packaging
- 1g
- Price
- $350
- Updated
- 2021/12/16
N-ETHYL-N-(4-FLUOROPHENYL)AMINE Chemical Properties,Usage,Production
Synthesis
121-44-8
371-40-4
405-67-4
The general procedure for the synthesis of N-ethyl-4-fluoroaniline from triethylamine and 4-fluoroaniline is as follows: first, a mixed solution of IrCl3 (2 mol%, 0.02 mmol), ligand L1 (2.4 mol%, 0.024 mmol), sodium hydroxide (0.20 mmol), and xylene (3 mL) was stirred for 1 hr at room temperature in a Schlenk tube . Subsequently, 4-fluoroaniline (1.00 mmol), triethylamine (1.0 mL) and sodium hydroxide (1.00 mmol) were added to the reaction system. The reaction mixture was heated at 150 °C for 20 h, after which it was cooled to room temperature. Upon completion of the reaction, the resulting solution was purified directly by column chromatography using petroleum ether/ethyl acetate (10:1) as eluent to give the final target product N-ethyl-4-fluoroaniline (3a).
References
[1] ACS Catalysis, 2014, vol. 4, # 11, p. 3910 - 3918
[2] Tetrahedron Letters, 2016, vol. 57, # 41, p. 4588 - 4591
N-ETHYL-N-(4-FLUOROPHENYL)AMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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