5-CHLORO-2-IODOPHENOL
- Product Name
- 5-CHLORO-2-IODOPHENOL
- CAS No.
- 136808-72-5
- Chemical Name
- 5-CHLORO-2-IODOPHENOL
- Synonyms
- 5-CHLORO-2-IODOPHENO;2-Iodo-5-chlorophenol;5-CHLORO-2-IODOPHENOL;Phenol, 5-chloro-2-iodo-
- CBNumber
- CB11496249
- Molecular Formula
- C6H4ClIO
- Formula Weight
- 254.45
- MOL File
- 136808-72-5.mol
5-CHLORO-2-IODOPHENOL Property
- Boiling point:
- 219℃
- Density
- 2.087
- Flash point:
- 86℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 7.55±0.10(Predicted)
- form
- tiny crystals
- color
- Golden brown & dark tan
Safety
- HS Code
- 2908190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C371603
- Product name
- 5-Chloro-2-iodophenol
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 2601-M-01
- Product name
- 5-Chloro-2-iodophenol
- Packaging
- 1g
- Price
- $61
- Updated
- 2021/12/16
- Product number
- FC140714
- Product name
- 5-Chloro-2-iodophenol
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FC140714
- Product name
- 5-Chloro-2-iodophenol
- Packaging
- 1g
- Price
- $111
- Updated
- 2021/12/16
- Product number
- 119458
- Product name
- 5-Chloro-2-iodophenol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $134
- Updated
- 2021/12/16
5-CHLORO-2-IODOPHENOL Chemical Properties,Usage,Production
Synthesis
28443-50-7
136808-72-5
General procedure for the synthesis of 5-chloro-2-iodophenol from 2-amino-5-chlorophenol: 2-amino-5-chlorophenol (5.7 g, 40 mmol) was dissolved in a mixed solvent of DMSO/water/H2SO4 (200/60/140 mL) and the solution was cooled to 0 °C. A solution of sodium nitrite (4.1 g, 60 mmol) in water (20 mL) was slowly added at 0 °C and the reaction mixture was continuously stirred for 1 hour. Subsequently, a solution of potassium iodide (19.9 g, 120 mmol) in water (20 mL) was added to the reaction system and the mixture was stirred at room temperature for 1 hour. The same amount of potassium iodide (19.9 g, 120 mmol) in water (20 mL) solution was added again and the mixture continued to be stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was diluted with ethyl acetate and washed sequentially with water, saturated aqueous sodium sulfate solution and brine. The organic phase was dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The resulting residue was purified by fast chromatography (Biotage Si65M, 20% ethyl acetate/hexane) to afford 5-chloro-2-iodophenol 8.09 g (79% yield) as a pink solid. gC-MS m/e 254 [M]-.
References
[1] Patent: US2010/69425, 2010, A1. Location in patent: Page/Page column 11-12
[2] Journal of the Chemical Society, 1931, p. 2268,2271
5-CHLORO-2-IODOPHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-CHLORO-2-IODOPHENOL manufacturers
- Product
- 5-CHLORO-2-IODOPHENOL 136808-72-5
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 5-CHLORO-2-IODOPHENOL 136808-72-5
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09
- Product
- 5-CHLORO-2-IODOPHENOL 136808-72-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11