2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE

Product Name: 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE
CAS No.: 4761-00-6
Chemical Name: 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE
Synonyms: 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE;Benzene, 2-(bromomethyl)-1,3,5-trimethyl-
CBNumber: CB11564003
Molecular Formula: C10H13Br
Formula Weight: 213.11
MOL File: 4761-00-6.mol

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2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE Property

Melting point:: 50-51 °C
Boiling point:: 99-102 °C(Press: 2 Torr)
Density: 1.270±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to off-white Solid

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Safety

HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H319Causes serious eye irritation
Precautionary statements: P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B808160
Product name: 2-(Bromomethyl)-1,3,5-trimethylbenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 6497AB
Product name: 2-(Bromomethyl)-1,3,5-trimethylbenzene
Packaging: 25g
Price: $960
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0057365
Product name: 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE
Purity: 95.00%
Packaging: 2.5G
Price: $983.88
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0057365
Product name: 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE
Purity: 95.00%
Packaging: 5G
Price: $1168.42
Updated: 2021/12/16

AK Scientific

Product number: 6497AB
Product name: 2-(Bromomethyl)-1,3,5-trimethylbenzene
Packaging: 1g
Price: $100
Updated: 2021/12/16

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2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE Chemical Properties,Usage,Production

Uses

2-(Bromomethyl)-1,3,5-trimethylbenzene is a useful reactant for organic reactions and synthesis.

Synthesis

4170-90-5

4761-00-6

General procedure for the synthesis of 2,4,6-trimethylbenzyl bromide from 2,4,6-trimethylbenzyl alcohol: 2,4,6-trimethylbenzyl alcohol (0.6 g, 0.6 mmol) and methylene chloride (5 mL) were added to a round bottom flask. After stirring for 10 min, oxalyl chloride or oxalyl bromide (0.6 mmol) was slowly added. The reaction mixture was stirred magnetically at room temperature until gas release essentially ceased. Subsequently, 2,4,6-trimethylbenzyl alcohol (0.5 mmol) was added and the reaction mixture was heated to reflux. The progress of the reaction was monitored by TLC and upon completion of the reaction, the mixture was cooled to room temperature and filtered. The solid on the funnel was washed with dichloromethane (3 x 10 mL), the filtrate was combined and concentrated under reduced pressure. The purity of the resulting product 2,4,6-trimethylbenzyl bromide was confirmed by 1H NMR and 13C NMR spectral analysis.

References

[1] Beilstein Journal of Organic Chemistry, 2014, vol. 10, p. 1397 - 1405
[2] Organic Letters, 2009, vol. 11, # 2, p. 469 - 472
[3] Organic Letters, 2011, vol. 13, # 19, p. 5370 - 5373
[4] Journal of the American Chemical Society, 2018, vol. 140, # 32, p. 10099 - 10103
[5] Organic Letters, 2002, vol. 4, # 11, p. 1975 - 1977

2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE Suppliers

China 52 India 1 United States 4 Global 57

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View Lastest Price from 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE manufacturers

Hebei Zhuanglai Chemical Trading Co Ltd

Product: 2-Bromomethyl-1,3,5-trimethylbenzene 4761-00-6
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99
Supply Ability: 5000
Release date: 2024-11-13

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Bromomethyl-1,3,5-trimethylbenzene 4761-00-6
Price: US $1.00-22.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100000KG
Release date: 2024-07-08

Career Henan Chemical Co

Product: 2-(Bromomethyl)-1,3,5-trimethylbenzene 4761-00-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons
Release date: 2020-02-14

4761-00-6, 2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENERelated Search:

TRIMETHYLSILANE

2-(BROMOMETHYL)-1,3,5-TRIMETHYLBENZENE

Benzene, 2-(bromomethyl)-1,3,5-trimethyl-

4761-00-6