4,4'-DICHLOROBUTYROPHENONE
- Product Name
- 4,4'-DICHLOROBUTYROPHENONE
- CAS No.
- 40877-09-6
- Chemical Name
- 4,4'-DICHLOROBUTYROPHENONE
- Synonyms
- 4-chloro-1-(4-chlorophenyl)butan-1-one;butan-1-one;LABOTEST-BB LT00848184;4',γ-Dichlorobutyrophenone;4,4'-Dichlorobutyrophenone;4,4'-DICHLOROBUTYROPHENONE;4-Chloro-1-(4-chlorophenyl);GAMMA,4-DICHLOROBUTYROPHENONE;GAMMA,P-DICHLOROBUTYROPHENONE;4,4'-Dichlorobutyrophenone,97%
- CBNumber
- CB1156533
- Molecular Formula
- C10H10Cl2O
- Formula Weight
- 217.09
- MOL File
- 40877-09-6.mol
4,4'-DICHLOROBUTYROPHENONE Property
- Melting point:
- 29-30 °C
- Boiling point:
- 153-155 °C(Press: 2 Torr)
- Density
- 1.2372 (estimate)
- refractive index
- 1.5600
- form
- Pellets
- color
- White
- BRN
- 879782
- CAS DataBase Reference
- 40877-09-6(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- S535583
- Product name
- 4,4'-DICHLOROBUTYROPHENONE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $30.7
- Updated
- 2025/07/31
- Product number
- S535583
- Product name
- 4,4''-DICHLOROBUTYROPHENONE
- Purity
- AldrichCPR
- Packaging
- 250MG
- Price
- $29.8
- Updated
- 2024/03/01
- Product number
- 6031c
- Product name
- 4-chloro-1-(4-chlorophenyl)-1-oxobutane
- Purity
- 97%
- Packaging
- 1g
- Price
- $215
- Updated
- 2021/12/16
- Product number
- 103690
- Product name
- 4-Chloro-1-(4-chlorophenyl)-1-oxobutane
- Packaging
- 25g
- Price
- $245
- Updated
- 2021/12/16
- Product number
- 6031c
- Product name
- 4-chloro-1-(4-chlorophenyl)-1-oxobutane
- Purity
- 97%
- Packaging
- 2g
- Price
- $366
- Updated
- 2021/12/16
4,4'-DICHLOROBUTYROPHENONE Chemical Properties,Usage,Production
Chemical Properties
clear yellow to brown liquid after melting
Synthesis
29480-09-9
40877-09-6
To a dry reaction tube were sequentially added 0.2 mmol 1-(4-chlorophenyl)cyclobutanol, 0.02 mmol manganese dichloride (MnCl2), 0.6 mmol trimethylsilyl chloride (TMSCl), 0.4 mmol 2-iodobenzoic acid and 1 mL acetonitrile (MeCN). The reaction mixture was stirred at 50°C for 7 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The crude product was purified by column chromatography using a solvent mixture of petroleum ether and ethyl acetate as eluent (20:1 v/v). The final product was 4,4'-dichlorobutyrophenone in 88.2% yield and 98% purity.
References
[1] Organic Letters, 2016, vol. 18, # 4, p. 684 - 687
[2] Patent: CN106008181, 2016, A. Location in patent: Paragraph 0039-0041
4,4'-DICHLOROBUTYROPHENONE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4,4'-DICHLOROBUTYROPHENONE manufacturers
- Product
- 4,4"-DICHLOROBUTYROPHENONE 40877-09-6
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11