3-PHENYL-4-PICOLINE
- Product Name
- 3-PHENYL-4-PICOLINE
- CAS No.
- 19352-29-5
- Chemical Name
- 3-PHENYL-4-PICOLINE
- Synonyms
- 3-PHENYL-4-PICOLINE;4-METHYL-3-PHENYLPYRIDINE;Pyridine, 4-methyl-3-phenyl-
- CBNumber
- CB1159453
- Molecular Formula
- C12H11N
- Formula Weight
- 169.22
- MOL File
- 19352-29-5.mol
3-PHENYL-4-PICOLINE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M356418
- Product name
- 4-Methyl-3-phenylpyridine
- Packaging
- 50mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- Z0323
- Product name
- 4-Methyl-3-phenylpyridine
- Packaging
- 250mg
- Price
- $158
- Updated
- 2021/12/16
- Product number
- CHM0012009
- Product name
- 4-METHYL-3-PHENYLPYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.22
- Updated
- 2021/12/16
- Product number
- CM122472
- Product name
- 4-methyl-3-phenylpyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $561
- Updated
- 2021/12/16
- Product number
- 25177
- Product name
- 4-Methyl-3-phenylpyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $564
- Updated
- 2021/12/16
3-PHENYL-4-PICOLINE Chemical Properties,Usage,Production
Synthesis
72093-04-0
100-58-3
19352-29-5
Pd Catalyst 1 (12.6 mg, 0.045 mmol, calculated based on the molar concentration of Pd) and 3-chloro-4-methylpyridine (0.2 mmol) were added to a Schlenk tube equipped with a magnetic stir bar. Anhydrous toluene (2.0 mL) and phenylmagnesium bromide (0.3 mmol, 1.5 equiv) were added sequentially under nitrogen protection. The reaction mixture was heated to 140 °C and the reaction was stirred at this temperature until complete consumption of 3-chloro-4-methylpyridine was confirmed by thin layer chromatography (TLC) monitoring. Upon completion of the reaction, the reaction mixture was purified by silica gel column chromatography to afford the target product 3-phenyl-4-methylpyridine.
References
[1] Tetrahedron, 2016, vol. 72, # 1, p. 69 - 75
3-PHENYL-4-PICOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
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