ChemicalBook > CAS DataBase List > N-(PHENYLTHIO)PHTHALIMIDE
N-(PHENYLTHIO)PHTHALIMIDE
- Product Name
- N-(PHENYLTHIO)PHTHALIMIDE
- CAS No.
- 14204-27-4
- Chemical Name
- N-(PHENYLTHIO)PHTHALIMIDE
- Synonyms
- N-(PHENYLTHIO)PHTHALIMIDE;N-(Phenylthio)phthalimide>N-(Phenylthio)phthalimide;2-(Phenylthio)isoindoline-1,3-dione;2-(Phenylthio)-1,3-isoindolinedione;2-(Phenylthio)-1H-isoindol-1,3(2H)-dione;2-(Phenylthio)-1H-isoindole-1,3(2H)-dione;1H-Isoindole-1,3(2H)-dione, 2-(phenylthio)-
- CBNumber
- CB1240906
- Molecular Formula
- C14H9NO2S
- Formula Weight
- 255.29
- MOL File
- 14204-27-4.mol
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N-(PHENYLTHIO)PHTHALIMIDE Property
- Melting point:
- 160-163 °C(lit.)
- Boiling point:
- 432.2±28.0 °C(Predicted)
- Density
- 1.42±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- DMSO: soluble25mg/mL, clear, yellow
- pka
- -3.05±0.20(Predicted)
- form
- powder to crystal
- color
- White to Light yellow
- CAS DataBase Reference
- 14204-27-4
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Safety
- Safety Statements
- 24/25
- WGK Germany
- 3
- HS Code
- 29309090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TCI Chemical
- Product number
- P1254
- Product name
- N-(Phenylthio)phthalimide
- Purity
- >98.0%(GC)(N)
- Packaging
- 5g
- Price
- $106
- Updated
- 2025/07/31
TCI Chemical
- Product number
- P1254
- Product name
- N-(Phenylthio)phthalimide
- Purity
- >98.0%(GC)(N)
- Packaging
- 25g
- Price
- $421
- Updated
- 2025/07/31
TRC
- Product number
- P399325
- Product name
- N-(Phenylthio)phthalimide
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
AK Scientific
- Product number
- 8363AL
- Product name
- N-(Phenylthio)phthalimide
- Packaging
- 1g
- Price
- $84
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0156787
- Product name
- N-(PHENYLTHIO)PHTHALIMIDE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $880.94
- Updated
- 2021/12/16
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N-(PHENYLTHIO)PHTHALIMIDE Chemical Properties,Usage,Production
Uses
Used as a mild sulfenylating reagent.
Preparation
?N-(Phenylthio)phthalimide is prepared by reaction of Benzenesulfenyl Chloride with Phthalimide in the presence of Triethylamine.
Preparation
(a) Preparation of benzenesulfenyl chloride. To a stirred solution of 55 gm (0.5 mole) of benzene thiol in 300 ml of η -pentane at 0°C is added chlorine gas until an assay (GC) of the resulting red-orange solution shows quantitative conversion to the sulfenyl chloride. The reaction usually requires about 39 gm (0.6 mole) of chlorine.
(b) Reaction of benzenesulfenyl chloride with phthalimide. To a stirred solution of 73.5 gm (0.5 mole) of phthalimide in 200 ml of dimethylforma-mide is first added 60 gm (0.6 mole) of triethylamine. Then the sulfenyl chloride solution from (a) is slowly added dropwise. The reaction mixture is stirred for \ hr, poured into 2 liters of cold water, filtered, and dried to afford 121 gm (95%), m.p. 160-161°C (recrystallized from ethanol).
Complex imides such as camphorimide and 9,10-dihydroanthracene-9,10-endo-a,/3-succinimide have been alkylated in methylene dichloride with alkyl halides, using tetrabutylammonium bromide as a phase-transfer catalyst and aqueous potassium hydroxide as a base.
N-(PHENYLTHIO)PHTHALIMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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