4-(2-BOC-AMINOETHYL)BENZOIC ACID
- Product Name
- 4-(2-BOC-AMINOETHYL)BENZOIC ACID
- CAS No.
- 132690-91-6
- Chemical Name
- 4-(2-BOC-AMINOETHYL)BENZOIC ACID
- Synonyms
- 4-(2-BOC-AMINOETHYL)BENZOIC ACID;4-
(2- Boc- aminoethyl) benzoic acid;4-[2-[(2-methylpropan-2-yl)oxycarbonylamino]ethyl]benzoic acid;Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]- - CBNumber
- CB1241024
- Molecular Formula
- C14H19NO4
- Formula Weight
- 265.3
- MOL File
- 132690-91-6.mol
4-(2-BOC-AMINOETHYL)BENZOIC ACID Property
- Boiling point:
- 440.5±38.0 °C(Predicted)
- Density
- 1.155±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 4.31±0.10(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B809888
- Product name
- 4-(2-((tert-Butoxycarbonyl)amino)ethyl)benzoicAcid
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 056447
- Product name
- 4-(2-{[(tert-Butoxy)carbonyl]amino}ethyl)-benzoic acid
- Purity
- >95%
- Packaging
- 500mg
- Price
- $244
- Updated
- 2021/12/16
- Product number
- X9841
- Product name
- 4-(2-Boc-aminoethyl)benzoicacid
- Packaging
- 5g
- Price
- $272
- Updated
- 2021/12/16
- Product number
- 056447
- Product name
- 4-(2-{[(tert-Butoxy)carbonyl]amino}ethyl)-benzoic acid
- Purity
- >95%
- Packaging
- 1g
- Price
- $304
- Updated
- 2021/12/16
- Product number
- CHM0068602
- Product name
- 4-(2-([(TERT-BUTOXY)CARBONYL]AMINO)ETHYL)BENZOIC ACID
- Purity
- 95.00%
- Packaging
- 500MG
- Price
- $720.84
- Updated
- 2021/12/16
4-(2-BOC-AMINOETHYL)BENZOIC ACID Chemical Properties,Usage,Production
Synthesis
24424-99-5
1199-69-5
132690-91-6
10A: 4-(2-aminoethyl)benzoic acid (200 mg, 0.99 mmol) and di-tert-butyl dicarbonate (260 mg, 1.2 mmol) were dissolved in 1 mL of 1 M NaOH aqueous solution. The reaction mixture was stirred at room temperature for 4 hours. Upon completion of the reaction, ethyl acetate was added followed by 10% aqueous citric acid solution. A white solid precipitate was observed, which was separated by filtration. The filtrate was extracted three times with ethyl acetate. The combined organic layers were washed sequentially with water and brine, dried over anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by rapid chromatography on silica gel with the eluent CH2Cl2/MeOH (100:0 to 95:5). A white solid product (47 mg, 16% yield) was obtained.1H NMR (CDCl3, ppm): δ 1.33 (s, 9H), 2.74 (t, J = 7.44 Hz, 2H), 3.14 (q, J = 6.78 Hz, 2H), 6.84 (br t, J = 5.43 Hz, 1H), 7.28 (d, J = 8.28 Hz, 2H ), 7.83 (d, J = 8.25 Hz, 2H).
References
[1] Patent: WO2012/3544, 2012, A1. Location in patent: Page/Page column 55
[2] Journal of Pharmacology and Experimental Therapeutics, 2008, vol. 324, # 1, p. 206 - 213
[3] Journal of Nanoscience and Nanotechnology, 2012, vol. 12, # 6, p. 5030 - 5038
[4] Patent: US2015/31673, 2015, A1. Location in patent: Paragraph 0409; 0410
4-(2-BOC-AMINOETHYL)BENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-(2-BOC-AMINOETHYL)BENZOIC ACID manufacturers
- Product
- 4-(2-Boc-aminoethyl)benzoic acid 132690-91-6
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99.4%
- Supply Ability
- 100 tons
- Release date
- 2022-01-25