DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE

Product Name: DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE
CAS No.: 909391-56-6
Chemical Name: DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE
Synonyms: )-benzyL;-[3-(4,4,5,5-tetramethyL;3-Dimethylaminomethylphenylboronic acid pinacol ester;3-(N,N-Dimethylaminomethyl)phenylboronic acid, pinacol ester;Benzenemethanamine, N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,...;Dimethyl({[3-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl})amine;DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE;Dimethyl[[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl]amine;N,N-dimethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine;Benzenemethanamine, N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
CBNumber: CB12448955
Molecular Formula: C15H24BNO2
Formula Weight: 261.17
MOL File: 909391-56-6.mol

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DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE Property

Boiling point:: 340.8±25.0 °C(Predicted)
Density: 1.00
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 8.78±0.28(Predicted)
Appearance: Colorless to off-white Solid-Liquid Mixture

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Safety

HS Code: 2931900090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: D479113
Product name: 3-(N,N-Dimethylaminomethyl)phenylboronicacid,pinacolester
Packaging: 250mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: BOR0004551
Product name: DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE
Purity: 95.00%
Packaging: 5G
Price: $2310
Updated: 2021/12/16

AK Scientific

Product number: AMTB764
Product name: 3-(Dimethylaminomethyl)phenylboronicacidpinacolester
Packaging: 1g
Price: $70
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8H60-1-B2
Product name: Dimethyl({[3-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl})amine
Packaging: 1g
Price: $128
Updated: 2021/12/16

Matrix Scientific

Product number: 096676
Product name: N,N-Dimethyl-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine
Purity: 95+%
Packaging: 500mg
Price: $142
Updated: 2021/12/16

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DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE Chemical Properties,Usage,Production

Synthesis

124-40-3

214360-74-4

909391-56-6

Step X1 Intermediate XI.1: 2-(3-(bromomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (297 mg, 1.0 mmol) was dissolved in acetonitrile (5 mL), a methanol solution of dimethylamine (2 M, 1.0 mL, 2.0 mmol) was added followed by potassium carbonate (691 mg, 5.0 mmol). The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, acetonitrile was removed under vacuum and the residue was partitioned with ethyl acetate and water. The organic layer was washed with saturated sodium bicarbonate solution, dried over magnesium sulfate, filtered and the filtrate was concentrated to afford dimethyl-[3-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)benzyl]amine (Intermediate XI.1) as a viscous oily substance (200 mg, 0.77 mmol, 77% yield). Characterization data for intermediate XI.1: 1H NMR (300 MHz, CD3OD): δ 7.70 (m, 2H), 7.30-7.45 (m, 2H), 3.50 (s, 2H), 2.28 (s, 6H), 1.36 (s, 12H) ppm; MS (ESI), m/z: 262 ([M + H]+).

References

[1] Patent: WO2006/95014, 2006, A1. Location in patent: Page/Page column 43-44

DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE Suppliers

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View Lastest Price from DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE manufacturers

Career Henan Chemical Co

Product: DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE 909391-56-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1kg; 10kg; 100kg
Release date: 2019-08-30

909391-56-6, DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINERelated Search:

4-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]MORPHOLINE 3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97% 3-(4-METHYLPIPERAZINE-1-CARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 1-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]PIPERIDINE 3-(PYRROLIDINE-1-CARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 3-(4-MORPHOLINOMETHYL)-PHENYLBORONIC ACID PINACOL ESTER HYDROCHLORIDE 3-[3-(ETHOXYCARBONYL)PIPERIDINE-1-CARBONYL]BENZENEBORONIC ACID PINACOL ESTER 3-(4-BOC-PIPERAZINE-1-CARBONYL)BENZENEBORONIC ACID PINACOL ESTER 1,2,3,4-TETRAHYDRO-2-METHYL-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-ISOQUINOLINE (2-(benzyloxy)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)(pyrrolidin-1-yl)methanone (3-PHTHALIMIDOMETHYLPHENYL)BORONIC ACID PINACOL ESTER 3-((N,N-DIMETHYLAMINO)METHY)PHENYL BORONIC ACID PINACOL ESTER HYDROCHLORIDE 4-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzoyl]morpholine 1-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]pyrrolidine 4-(N,N-DIETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 3-(PIPERIDINE-1-CARBONYL)PHENYLBORONIC ACID, PINACOL ESTER PIPERIDINOMETHYL-3-PHENYLBORONIC ACID PINACOL ESTER HYDROCHLORIDE

DIMETHYL-[3-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-BENZYL]-AMINE

3-(N,N-Dimethylaminomethyl)phenylboronic acid, pinacol ester

3-Dimethylaminomethylphenylboronic acid pinacol ester

Dimethyl[[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl]amine

3-Dimethylaminomethylphenylboronic acid pinacol ester Dimethyl[[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl]amine

N,N-dimethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine

N,N-Dimethyl-1-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methylamine

N,N-diMethyl-1-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)MethanaMine

Dimethyl({[3-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl})amine

Benzenemethanamine, N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

)-benzyL

-[3-(4,4,5,5-tetramethyL

Benzenemethanamine, N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,...

N,N-Dimethyl-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine - [D26397]

909391-56-6