ChemicalBook > CAS DataBase List > 7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE

7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE

Product Name: 7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
CAS No.: 894852-01-8
Chemical Name: 7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
Synonyms: 7-BroMo-2,2-diMethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one;7-Bromo-2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H);7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE;2H-Pyrido[3,2-b]-1,4-oxazin-3(4H)-one, 7-bromo-2,2-dimethyl-
CBNumber: CB12457416
Molecular Formula: C9H9BrN2O2
Formula Weight: 257.08
MOL File: 894852-01-8.mol

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7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE Property

Boiling point:: 380℃
Density: 1.533
Flash point:: 184℃
storage temp.: Sealed in dry,Room Temperature
pka: 10.05±0.40(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0368208
Product name: 7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
Purity: 95.00%
Packaging: 250MG
Price: $484.05
Updated: 2021/12/16

Matrix Scientific

Product number: 181641
Product name: 7-Bromo-2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one
Purity: 95%
Packaging: 5g
Price: $1156
Updated: 2021/12/16

Alichem

Product number: 894852018
Product name: 7-Bromo-2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 10g
Price: $1851.2
Updated: 2021/12/16

A1 Biochem Labs

Product number: 6570633
Product name: 7-Bromo-2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one
Purity: 95%
Packaging: 5G
Price: $700
Updated: 2021/12/16

Alichem

Product number: 894852018
Product name: 7-Bromo-2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one
Packaging: 5g
Price: $1042.72
Updated: 2021/12/16

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7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE Chemical Properties,Usage,Production

Synthesis

20348-21-4

894852-01-8

Step (ii): Synthesis of 7-bromo-2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one (Intermediate-18) To a stirred solution of 2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)-one (18.1) (2 g, 11.23 mmol) in dichloromethane (DCM) (20 mL) was added sodium carbonate (Na2CO3) (3.57 g, 33.70 mmol) and bromine (0.92 mL, 17.97 mmol) in turn at 0°C. The solution was purified with aqueous solution of sodium carbonate (Na2CO3) (3.57 g, 33.70 mmol). 17.97 mmol). The reaction mixture was stirred at 20-35°C for 16 hours. Upon completion of the reaction, the reaction mixture was diluted with ice water, the resulting solid was collected by filtration and washed with cold water to afford the target compound as a white solid (1.8 g, 86% yield).1H NMR (400 MHz, DMSO-d6) data were consistent with the expected structure.

References

[1] Patent: WO2015/71780, 2015, A1. Location in patent: Page/Page column 22

7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE Suppliers

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894852-01-8, 7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONERelated Search:

7-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE

7-Bromo-2,2-dimethyl-2H-pyrido[3,2-b][1,4]oxazin-3(4H)

7-BroMo-2,2-diMethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one

2H-Pyrido[3,2-b]-1,4-oxazin-3(4H)-one, 7-bromo-2,2-dimethyl-

894852-01-8