5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL

Product Name: 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL
CAS No.: 33781-38-3
Chemical Name: 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL
Synonyms: 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL
CBNumber: CB12458266
Molecular Formula: C9H9ClO
Formula Weight: 168.62
MOL File: 33781-38-3.mol

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5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL Property

Boiling point:: 292.7±35.0 °C(Predicted)
Density: 1.322±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.02±0.20(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C433248
Product name: 5-Chloro-2,3-dihydro-1H-inden-1-ol
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 3977AB
Product name: 5-Chloro-2,3-dihydro-1H-inden-1-ol
Packaging: 250mg
Price: $158
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367190
Product name: 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL
Purity: 95.00%
Packaging: 5MG
Price: $495.33
Updated: 2021/12/16

Crysdot

Product number: CD12082006
Product name: 5-Chloro-2,3-dihydro-1H-inden-1-ol
Purity: 95+%
Packaging: 10g
Price: $557
Updated: 2021/12/16

Alichem

Product number: 33781383
Product name: 5-Chloro-2,3-dihydro-1H-inden-1-ol
Packaging: 10g
Price: $613.67
Updated: 2021/12/16

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5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL Chemical Properties,Usage,Production

Synthesis

42348-86-7

33781-38-3

To a solution of 5-chloro-1-indanone (500 g, 301.2 mmol) in tetrahydrofuran (THF, 500 mL), an aqueous solution (100 mL) of sodium borohydride (23.0 g, 602.4 mmol) was slowly added dropwise at a controlled temperature of between 0 °C and 100 °C for 1 hour. The reaction mixture was stirred at room temperature for 12 hours. After completion of the reaction, the reaction was quenched with water (500 mL) and extracted with ethyl acetate (3 x 1500 mL). The organic layers were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure to afford a racemic mixture of 5-chloro-2,3-dihydro-1H-inden-1-ol (48.0 g, 94.8% yield), which can be used directly in the next step of the reaction without further purification.

References

[1] Journal of the American Chemical Society, 2005, vol. 127, # 30, p. 10482 - 10483
[2] Patent: WO2017/147410, 2017, A1. Location in patent: Page/Page column 134; 135
[3] Bulletin de la Societe Chimique de France, 1973, p. 3096 - 3099
[4] Journal of Medicinal Chemistry, 2005, vol. 48, # 5, p. 1563 - 1575
[5] Journal of Medicinal Chemistry, 2005, vol. 48, # 6, p. 1796 - 1805

5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL Suppliers

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View Lastest Price from 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL 33781-38-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-08-15

33781-38-3, 5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OLRelated Search:

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5-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL

33781-38-3