2-CHLORO-4-METHOXYNITROBENZENE
- Product Name
- 2-CHLORO-4-METHOXYNITROBENZENE
- CAS No.
- 28987-59-9
- Chemical Name
- 2-CHLORO-4-METHOXYNITROBENZENE
- Synonyms
- APAZ-004;2-Chloro-4-methoxynitro;Anisole, 3-chloro-4-nitro-;Benzene, 2-chloro-4-methoxy-1-nitro-;2-CHLORO-4-METHOXY-1 NITROBENZENE (5GMS);2-CHLORO-4-METHOXY-1 NITROBENZENE (220 G
- CBNumber
- CB12460591
- Molecular Formula
- C7H6ClNO3
- Formula Weight
- 187.58
- MOL File
- 28987-59-9.mol
2-CHLORO-4-METHOXYNITROBENZENE Property
- Density
- 1.366
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to yellow Solid
Safety
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H313May be harmful in contact with skin
H317May cause an allergic skin reaction
H373May cause damage to organs through prolonged or repeated exposure
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P270Do not eat, drink or smoke when using this product.
P272Contaminated work clothing should not be allowed out of the workplace.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P314Get medical advice/attention if you feel unwell.
P330Rinse mouth.
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P363Wash contaminated clothing before reuse.
P403Store in a well-ventilated place.
N-Bromosuccinimide Price
- Product number
- C596808
- Product name
- 2-Chloro-4-methoxy-1-nitrobenzene
- Packaging
- 500mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 120035
- Product name
- 2-Chloro-4-methoxy-1-nitrobenzene
- Purity
- 95+%
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- FC146930
- Product name
- 2-Chloro-4-methoxy-1-nitrobenzene
- Packaging
- 25mg
- Price
- $185
- Updated
- 2021/12/16
- Product number
- FC146930
- Product name
- 2-Chloro-4-methoxy-1-nitrobenzene
- Packaging
- 5mg
- Price
- $53
- Updated
- 2021/12/16
- Product number
- FC146930
- Product name
- 2-Chloro-4-methoxy-1-nitrobenzene
- Packaging
- 10mg
- Price
- $93
- Updated
- 2021/12/16
2-CHLORO-4-METHOXYNITROBENZENE Chemical Properties,Usage,Production
Synthesis
1882-69-5
28987-59-9
General procedure for the synthesis of 2-chloro-4-methoxynitrobenzene from 5-methoxy-2-nitrobenzoic acid: to a Silak reaction tube equipped with a magnetic stirrer, 6.2 mg of silver sulfate, 36.3 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline, 39.4 mg of 5-methoxy-2-nitrobenzoic acid and 17.5 mg of NaCl, dissolved in 4 mL of dimethyl sulfoxide. The reaction system was heated at 160°C for 24 hours under oxygen atmosphere. After completion of the reaction, the reaction was quenched by addition of distilled water and extracted with ethyl acetate three times at 10 mL each. the organic phases were combined and concentrated to give 25.1 mg of 2-chloro-4-methoxynitrobenzene in 67% yield.
References
[1] Tetrahedron Letters, 2010, vol. 51, # 50, p. 6646 - 6648
[2] Journal of Organic Chemistry, 2016, vol. 81, # 7, p. 2794 - 2803
[3] Patent: CN107325002, 2017, A. Location in patent: Paragraph 0133
[4] Organic and Biomolecular Chemistry, 2018, vol. 16, # 30, p. 5416 - 5421
2-CHLORO-4-METHOXYNITROBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-CHLORO-4-METHOXYNITROBENZENE manufacturers
- Product
- 2-CHLORO-4-METHOXYNITROBENZENE 28987-59-9
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-12
- Product
- 3-Chloro-4-nitroanisole 28987-59-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2018-12-25