SINOVA SL-03967
- Product Name
- SINOVA SL-03967
- CAS No.
- 107259-05-2
- Chemical Name
- SINOVA SL-03967
- Synonyms
- SINOVA SL-03967;Ethyl 1-(Boc-aMino)cyclopropanecarboxylate;1-N-(BOC)AMino-cyclopropane-1-carboxylic acid ethyl ester;Ethyl 1-((tert-butoxycarbonyl)aMino)cyclopropanecarboxylate;ethyl 1-((tert-butoxycarbonyl)amino)cyclopropane-1-carboxylate;Ethyl 1-[(2-methylpropan-2-yl)oxycarbonylamino]cyclopropane-1-carboxylate;Ethyl1-((tert-butoxycarbonyl)amino)cyclopropanecarboxylate CAS：107259-05-2;1-[[(1,1-dimethylethoxy)carbonyl]amino]Cyclopropane carboxylic acid Ethyl ester;Cyclopropanecarboxylic acid, 1-[[(1,1-diMethylethoxy)carbonyl]aMino]-, ethyl ester
- CBNumber
- CB12464812
- Molecular Formula
- C11H19NO4
- Formula Weight
- 229.27
- MOL File
- 107259-05-2.mol
SINOVA SL-03967 Property
- Melting point:
- 44-46 °C(Solv: pentane (109-66-0))
- Boiling point:
- 307.0±21.0 °C(Predicted)
- Density
- 1.10±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 10.87±0.20(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- E921683
- Product name
- Ethyl1-((tert-Butoxycarbonyl)amino)cyclopropanecarboxylate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CHM0125151
- Product name
- 1-N-(BOC)AMINO-CYCLOPROPANE-1-CARBOXYLIC ACID ETHYL ESTER
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.41
- Updated
- 2021/12/16
- Product number
- A-1626
- Product name
- Ethyl1-(Boc-amino)-cyclopropanecarboxylate
- Purity
- 97%
- Packaging
- 1g
- Price
- $129.62
- Updated
- 2021/12/16
- Product number
- CM202801
- Product name
- ethyl1-((tert-butoxycarbonyl)amino)cyclopropane-1-carboxylate
- Purity
- 95%
- Packaging
- 5g
- Price
- $196
- Updated
- 2021/12/16
- Product number
- CD21019027
- Product name
- Ethyl1-((tert-butoxycarbonyl)amino)cyclopropanecarboxylate
- Purity
- 95+%
- Packaging
- 10g
- Price
- $315
- Updated
- 2021/12/16
SINOVA SL-03967 Chemical Properties,Usage,Production
Synthesis
24424-99-5
42303-42-4
107259-05-2
The general procedure for the synthesis of ethyl 1-(BOC-amino)cyclopropane-1-carboxylate from di-tert-butyl dicarbonate and ethyl 1-aminocyclopropane-1-carboxylate hydrochloride was as follows: to a solution of 1-aminocyclopropane carboxylic acid ethyl ester hydrochloride (3.22 g, 19.4 mmol) in dichloromethane (35 mL) was added triethylamine (2.71 mL, 19.4 mmol) to form a suspension. A solution of dichloromethane (5 mL) of di-tert-butyl dicarbonate (4.24 g, 19.4 mmol) was added slowly and dropwise over about 5 hours. The reaction mixture was stirred overnight at room temperature. After completion of the reaction, extraction was carried out by adding 1 M aqueous KHSO4 solution (100 mL) and dichloromethane (50 mL). The organic layer was separated, dried over anhydrous sodium sulfate, the solvent was evaporated under reduced pressure and co-evaporated with tetrahydrofuran (2×) to give 4.31 g (97% yield) of ethyl 1-(BOC-amino)cyclopropanecarboxylate.
References
[1] Patent: WO2015/90603, 2015, A1. Location in patent: Page/Page column 59; 60
[2] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 7, p. 2151 - 2155
SINOVA SL-03967 Preparation Products And Raw materials
Raw materials
Preparation Products
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