ChemicalBook > CAS DataBase List > Methyl 4-(N-phenylcaramoyl)benzoate

Methyl 4-(N-phenylcaramoyl)benzoate

Product Name: Methyl 4-(N-phenylcaramoyl)benzoate
CAS No.: 3814-10-6
Chemical Name: Methyl 4-(N-phenylcaramoyl)benzoate
Synonyms: BA-MMT;N-phenyl-p-carbomethoxybenzamide;Methyl 4-(phenylcarbaMoyl)benzoate;Methyl 4-(anilinocarbonyl)benzoate;METHYL 4-(N-PHENYLCARBAMOYL)BENZOATE;Methyl 4-(N-phenylcaramoyl)benzoate;Methyl 4-(Phenylcarbamoyl)benzoate >4-(Phenylcarbamoyl)benzoic Acid Methyl Ester;4-[(phenylamino)carbonyl]Benzoic acid methyl ester;Benzoic acid, 4-[(phenylamino)carbonyl]-, methyl ester
CBNumber: CB12473803
Molecular Formula: C15H13NO3
Formula Weight: 255.27
MOL File: 3814-10-6.mol

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Methyl 4-(N-phenylcaramoyl)benzoate Property

Melting point:: 193℃
Density: 1.237
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
color: White to Almost white
CAS DataBase Reference: 3814-10-6

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Safety

HS Code: 2924.29.7790

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: M2637
Product name: Methyl 4-(Phenylcarbamoyl)benzoate
Purity: >98.0%(GC)
Packaging: 1g
Price: $52
Updated: 2024/03/01

TCI Chemical

Product number: M2637
Product name: Methyl 4-(Phenylcarbamoyl)benzoate
Purity: >98.0%(GC)
Packaging: 5g
Price: $148
Updated: 2025/07/31

TRC

Product number: M339073
Product name: Methyl4-(N-Phenylcaramoyl)benzoate
Packaging: 500mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: X0043
Product name: Methyl4-(N-phenylcaramoyl)benzoate
Packaging: 5g
Price: $142
Updated: 2021/12/16

Ambeed

Product number: A141662
Product name: Methyl 4-(Phenylcarbamoyl)benzoate
Purity: 98%
Packaging: 25g
Price: $62
Updated: 2021/12/16

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Methyl 4-(N-phenylcaramoyl)benzoate Chemical Properties,Usage,Production

Chemical Properties

Grey white powder

Synthesis Reference(s)

The Journal of Organic Chemistry, 39, p. 3327, 1974 DOI: 10.1021/jo00937a004

Synthesis

7377-26-6

62-53-3

3814-10-6

To a 1 L three-necked round-bottomed flask equipped with a magnetic stirrer, a constant-pressure dropping funnel, an ice-water bath, a nitrogen protection system, a condenser tube, and a heating plate, 93.13 g of aniline, 42.30 g of sodium bicarbonate, 0.5 g of triethylamine, and 300 mL of tetrahydrofuran (THF) were added sequentially. The reaction mixture was cooled to below 10°C, followed by the slow dropwise addition of 100 g of methyl 4-chlorocarbonylbenzoate dissolved in 100 mL of THF. The reaction temperature was maintained at about 10°C during the dropwise addition.After the dropwise addition was completed, the reaction mixture was heated to reflux and the progress of the reaction was monitored by infrared spectroscopy (IR) (disappearance of the characteristic peak at 1780 cm-1 indicated completion of the reaction). After completion of the reaction, the reaction solution was diluted to 2 L with cold deionized water and stirring was continued for about 20 min. The solid product was collected by filtration and dried in an oven at 110°C. A final product of 105.6 g of the target product 4-methoxycarbonylbenzanilide was obtained in 82.2% yield.

References

[1] Patent: WO2015/42561, 2015, A1. Location in patent: Paragraph 0124
[2] Patent: WO2015/42563, 2015, A1. Location in patent: Paragraph 0124
[3] Patent: US9200142, 2015, B2. Location in patent: Page/Page column 36

Methyl 4-(N-phenylcaramoyl)benzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 4-(N-phenylcaramoyl)benzoate manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Methyl 4-(N-phenylcaramoyl)benzoate 3814-10-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20t
Release date: 2024-07-16

Shaanxi Dideu Medichem Co. Ltd

Product: Methyl 4-(N-phenylcaraMoyl)benzoate 3814-10-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2019-12-31

3814-10-6, Methyl 4-(N-phenylcaramoyl)benzoateRelated Search:

Methyl 4-(N-phenylcaramoyl)benzoate

METHYL 4-(N-PHENYLCARBAMOYL)BENZOATE

Methyl 4-(anilinocarbonyl)benzoate

Methyl 4-(phenylcarbaMoyl)benzoate

BA-MMT

4-[(phenylamino)carbonyl]Benzoic acid methyl ester

N-phenyl-p-carbomethoxybenzamide

Methyl 4-(Phenylcarbamoyl)benzoate &gt

Benzoic acid, 4-[(phenylamino)carbonyl]-, methyl ester

4-(Phenylcarbamoyl)benzoic Acid Methyl Ester

3814-10-6