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2-(1H-indol-3-yl)-2-methylpropan-1-amine

Product Name
2-(1H-indol-3-yl)-2-methylpropan-1-amine
CAS No.
15467-31-9
Chemical Name
2-(1H-indol-3-yl)-2-methylpropan-1-amine
Synonyms
beta,beta-Dimethyltryptamine;3-(2-Amino-tert-butyl)indole;1H-Indole-3-ethanamine, β,β-dimethyl-;1H-Indole-3-ethanaMine, b,b-diMethyl-;2-(1H-indol-3-yl)-2-methylpropan-1-amine
CBNumber
CB12489747
Molecular Formula
C12H16N2
Formula Weight
188.27
MOL File
15467-31-9.mol
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2-(1H-indol-3-yl)-2-methylpropan-1-amine Property

Boiling point:
347.3±17.0 °C(Predicted)
Density 
1.093
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
17.31±0.30(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0097170
Product name
2-(1H-INDOL-3-YL)-2-METHYLPROPAN-1-AMINE
Purity
95.00%
Packaging
1G
Price
$2856
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0097170
Product name
2-(1H-INDOL-3-YL)-2-METHYLPROPAN-1-AMINE
Purity
95.00%
Packaging
5G
Price
$3811.5
Updated
2021/12/16
Alichem
Product number
15467319
Product name
2-(1H-Indol-3-yl)-2-methylpropan-1-amine
Packaging
250mg
Price
$183.6
Updated
2021/12/16
Abosyn
Product number
61-2526
Product name
2-(1H-Indol-3-yl)-2-methylpropan-1-amine
Purity
95%-98%
Packaging
0.25g
Price
$405
Updated
2021/12/16
Chemenu
Product number
CM148620
Product name
2-(1H-indol-3-yl)-2-methylpropan-1-amine
Purity
95%
Packaging
1g
Price
$421
Updated
2021/12/16
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2-(1H-indol-3-yl)-2-methylpropan-1-amine Chemical Properties,Usage,Production

Synthesis

23078-29-7

15467-31-9

2-(1H-indol-3-yl)-2-methylpropionitrile (1.8 g, 9.8 mmol) was dissolved in tetrahydrofuran (4 mL) at 25 °C, followed by the addition of methanol (10 mL) and Ruanne nickel catalyst (200 mg). The reaction was carried out under hydrogen pressure of 2.2 MPa for 72 hours. Upon completion of the reaction, the reaction was stopped and filtration was performed. The filtrate was concentrated by rotary evaporation under reduced pressure and subsequently purified by column chromatography with an eluent ratio of dichloromethane/methanol (v/v) = 20/1, which ultimately afforded the target product 2-(1H-indol-3-yl)-2-methyl-1-propanamine as a light yellow oil (1.58 g, 86% yield).

References

[1] Patent: CN104496987, 2016, B. Location in patent: Paragraph 0217; 0218; 0219; 0220
[2] Patent: CN104529865, 2017, B. Location in patent: Paragraph 0164; 0178; 0179
[3] Patent: WO2004/19935, 2004, A1. Location in patent: Page/Page column 67
[4] Journal of Medicinal Chemistry, 2009, vol. 52, # 4, p. 904 - 907

2-(1H-indol-3-yl)-2-methylpropan-1-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(1H-indol-3-yl)-2-methylpropan-1-amine Suppliers

China 14 United States 2 Global 16
Nanjing Vital Chemical Co., Ltd.
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15467-31-9, 2-(1H-indol-3-yl)-2-methylpropan-1-amineRelated Search:

Indole

  • 2-(1H-indol-3-yl)-2-methylpropan-1-amine
  • 1H-Indole-3-ethanaMine, b,b-diMethyl-
  • 3-(2-Amino-tert-butyl)indole
  • beta,beta-Dimethyltryptamine
  • 1H-Indole-3-ethanamine, β,β-dimethyl-
  • 15467-31-9