ChemicalBook > CAS DataBase List > 3-Fluoro-5-bromoaniline

3-Fluoro-5-bromoaniline

Product Name: 3-Fluoro-5-bromoaniline
CAS No.: 134168-97-1
Chemical Name: 3-Fluoro-5-bromoaniline
Synonyms: 3-BroMo-5-fluoro-phenylaMine;5-BroMo-3-fluoroaniline;3-Fluoro-5-bromoaniline;3-Bromo-5-fluoroaniline 97%;3-Bromo-5-fluorobenzenamine;3-Bromo-5-fluoroaniline,95%;Benzenamine, 3-bromo-5-fluoro-
CBNumber: CB12500057
Molecular Formula: C6H5BrFN
Formula Weight: 190.01
MOL File: 134168-97-1.mol

Less

3-Fluoro-5-bromoaniline Property

Boiling point:: 246℃
Density: 1.694
Flash point:: 102℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.51±0.10(Predicted)
form: Liquid
color: Brown
InChI: InChI=1S/C6H5BrFN/c7-4-1-5(8)3-6(9)2-4/h1-3H,9H2
InChIKey: NGZAVSDIXFIWHJ-UHFFFAOYSA-N
SMILES: C1(N)=CC(F)=CC(Br)=C1
CAS DataBase Reference: 134168-97-1

Less

Safety

RIDADR: UN2811
HazardClass: 6.1
HS Code: 2921420090

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

Less

N-Bromosuccinimide Price

TRC

Product number: B679178
Product name: 3-Bromo-5-fluoroaniline
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 074376
Product name: 3-Bromo-5-fluoroaniline
Purity: 95+%
Packaging: 1g
Price: $80
Updated: 2021/12/16

Apolloscientific

Product number: PC49300
Product name: 3-Bromo-5-fluoroaniline
Purity: 97%
Packaging: 5g
Price: $119
Updated: 2021/12/16

Apolloscientific

Product number: PC49300
Product name: 3-Bromo-5-fluoroaniline
Purity: 97%
Packaging: 1g
Price: $41
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3630-B-X4
Product name: 3-Bromo-5-fluoroaniline
Packaging: 1g
Price: $45
Updated: 2021/12/16

Less

3-Fluoro-5-bromoaniline Chemical Properties,Usage,Production

Synthesis

807620-95-7

134168-97-1

N-(3-bromo-5-fluorophenyl)acetamide (Intermediate 181, 8.7 g, 37.4 mmol) was used as a raw material, which was dissolved in ethanol (30 mL) and then concentrated hydrochloric acid (80 mL) was slowly added. The reaction mixture was heated to 100 °C and kept for 1 h for the reaction. After completion of the reaction, the mixture was cooled to room temperature and neutralized with 5 N sodium hydroxide solution. The crude product was extracted with ethyl acetate (2 x 100 mL) and the combined organic layers were washed with brine and dried over anhydrous magnesium sulfate. After filtration, the solvent was removed by concentration under reduced pressure. Purification by silica gel column chromatography using a gradient elution with 5-10% ethyl acetate in hexane solution gave 5.3 g (75% yield) of the yellow oily target product 3-bromo-5-fluoroaniline (Intermediate 180). Mass spectrum (ES+): m/z 190, 192 ([M+H]+), molecular formula C6H5BrFN. 1H NMR (DMSO-d6) δ: 5.46-6.00 (m, 2H), 6.24-6.37 (m, 1H), 6.44-6.53 (m, 1H), 6.54-6.61 (m, 1H).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2004, vol. 14, # 22, p. 5477 - 5480
[2] Bioorganic and Medicinal Chemistry Letters, 2005, vol. 15, # 22, p. 5061 - 5064
[3] Patent: WO2006/134378, 2006, A1. Location in patent: Page/Page column 149

3-Fluoro-5-bromoaniline Preparation Products And Raw materials

Raw materials

Preparation Products

Less

3-Fluoro-5-bromoaniline Suppliers

Canada 1 China 118 India 2 United Kingdom 1 United States 9 Global 131

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

Jalor-Chem co.,LTD

Tel: 0510-0510-86396359 13382276200
Email: sales@jalor-chem.com
Country: China
ProdList: 996
Advantage: 56

Shanghai Hongju Pharmaceutical Technology Co., LTD

Tel: 18001895509
Fax: QQ2934193566;
Email: 986383309@qq.com
Country: China
ProdList: 2680
Advantage: 58

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

Jia Xing Isenchem Co.,Ltd

Tel: 0573-85285100 18627885956
Fax: 0573-85285100
Email: isenchem@163.com
Country: China
ProdList: 9310
Advantage: 66

Accela ChemBio Co.,Ltd.

Tel: 021-50795510 4000665055
Fax: 021-50795055
Email: sales@accelachem.com
Country: China
ProdList: 11035
Advantage: 64

Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
Fax: 021-58099609
Email: bin.wu@shlschem.com
Country: China
ProdList: 9883
Advantage: 59

Shanghai Harvest Chemical Industrial Co., Ltd.

Tel: 021-31038972,31038973 17321035817
Fax: +86-21-51385350
Email: sales@harvest-chem.com
Country: China
ProdList: 2816
Advantage: 64

Nanjing Chemlin Chemical Co., Ltd

Tel: 025-83697070
Fax: +86-25-83453306
Email: info@chemlin.com.cn
Country: China
ProdList: 15883
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Shandong Xiya Chemical Co., Ltd

Tel: 4009903999 13355009207
Fax: 0539-6365991
Email: 3007715519@qq.com
Country: China
ProdList: 18729
Advantage: 57

Atop-Pharma (Shanghai) Technology Co., Ltd.

Tel: +86 (21) 5196-9732
Fax: +86 (21) 5196-9733
Country: China
ProdList: 996
Advantage: 57

Wuhan ariel chemical Co., LTD.

Tel: 18986259541
Fax: 027-87840182
Email: sales@3stc.com
Country: China
ProdList: 3763
Advantage: 58

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

Nanjing Norris-Pharm Technology Co., Ltd

Tel: 18652989687
Fax: +86-25-52131256
Email: sales@norris-pharm.com
Country: China
ProdList: 8878
Advantage: 55

Shanghai Jian Chao Chemical Technology Co., Ltd.

Tel: 150-2103-5486 18017383231
Fax: qq：2817624287
Email: 983544897@qq.com
Country: China
ProdList: 9342
Advantage: 55

9ding chemical ( Shanghai) Limited

Tel: 4009209199
Fax: 86-021-52271987
Email: sales@9dingchem.com
Country: China
ProdList: 18209
Advantage: 56

Shanghai Aladdin Bio-Chem Technology Co.,LTD

Tel: 400-6206333 13167063860
Fax: 021-50323701
Email: anhua.mao@aladdin-e.com
Country: China
ProdList: 25003
Advantage: 65

Shanghai Raise Chemical Technology Co.,Ltd

Tel: +86-021-50935922
Fax: +86-021-33847795
Country: China
ProdList: 7865
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Mashilabs (Shanghai) Co.,Ltd.

Tel: 19916721580
Fax: QQ：3154870176
Email: mafarm@126.com
Country: China
ProdList: 4542
Advantage: 58

Shanghai Jovan Biochemical Technology Co. Ltd.

Tel: +86-021-61654350
Fax: +86-021-61654350
Email: 1245958370@qq.com
Country: China
ProdList: 2982
Advantage: 50

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692 13912302692;
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

SanoChem (Chengdu) Tech. Co., Ltd.

Tel: 28-87999436 02887999436
Fax: QQ:2746983436
Email: sales@sano-chem.com
Country: China
ProdList: 3795
Advantage: 55

NovoChemy Ltd.

Tel: 86-(0)21-31261262 373522135
Fax: 86-(0)21-33250524
Email: sales@novochemy.com
Country: China
ProdList: 6498
Advantage: 58

Shanghai Shanyuan pharmaceutical technology co., LTD

Tel: 021-31761238 13167072949
Fax: 021-31761238
Email: 3146446224@qq.com
Country: China
ProdList: 1379
Advantage: 55

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

Changzhou Hopschain Chemical Co.,Ltd.

Tel: 0519-85528066 13775048983
Fax: 0519-85528066
Email: sales@hopschem.com
Country: China
ProdList: 31553
Advantage: 55

parabiochem

Tel: 025-83453382-8005
Fax: 025-83453382
Email: sale@parabiochem.com
Country: China
ProdList: 9595
Advantage: 55

Chengdu Huachun Technology Co., Ltd

Tel: 400-1166-196 15982826727
Fax: QQ：800101999
Email: cdhxsj@163.com
Country: China
ProdList: 14603
Advantage: 60

Shanghai Chaolan Chemical Technology Center

Tel: 021-QQ：65489617 15618227136
Fax: 21-5161 9052
Email: Sales@ATKchemical.com
Country: China
ProdList: 9125
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Zhengzhou Huiju Chemical Co., Ltd.

Tel: 0371-55900031 18137872243
Fax: QQ：2853979815
Email: 2853979815@qq.com
Country: China
ProdList: 9975
Advantage: 55

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Shanghai BaiShun Biological Technology Co., Ltd

Tel: 021-37581181
Fax: 021-57456066
Email: sales@chem-mall.com
Country: China
ProdList: 10330
Advantage: 58

Shanghai Zhen Li Biological Technology Co., Ltd

Tel: 021-16621358918; 18516310516
Fax: 13045646768
Email: zhenlipharma888@163.com
Country: China
ProdList: 19035
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 400821072
Fax: 021-58955996
Email: malulu@leyan.com
Country: China
ProdList: 25000
Advantage: 58

Suzhou Xiya Pharmaceutical Co., Ltd.

Tel: 0512-87819718 18912655635
Email: 2587879032@qq.com
Country: China
ProdList: 1401
Advantage: 58

Nanjing ChemLin Chemical Industry Co., Ltd.

Tel: 025-83453327
Fax: 025-83453327
Email: product@chemlin.com.cn
Country: China
ProdList: 277
Advantage: 58

3A Chemicals

Tel: 400-668-9898
Fax: 010-51582189
Email: service@3achem.com
Country: China
ProdList: 20557
Advantage: 58

DILICHEM

Tel: 0519-0519-81238123 18014346496
Email: shichaojun@126.com
Country: China
ProdList: 394
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000 13917643586;
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9856
Advantage: 58

Zhengzhou Acme Chemical Co., Ltd.

Tel: 0371-037163312495,13303845143 13303845143
Fax: QQ3001379618
Email: 3001379618@qq.com
Country: China
ProdList: 10267
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Xinyi Kaiwu Chemical Technology Co., Ltd.

Tel: 0516-0516-88997009 18651776937
Email: 4164357@qq.com
Country: China
ProdList: 3204
Advantage: 58

Shanghai Ze Chong Pharmaceutical Technology Co., Ltd.

Tel: 021-67308028 18621330623
Email: sales@zechongchem.com
Country: China
ProdList: 453
Advantage: 58

Allfluoro pharmaceutical co. ltd.

Tel: +86-400-0216110 +86-15958047586
Fax: 0086-21-33275002
Email: sales@allfluoro.com
Country: China
ProdList: 11385
Advantage: 58

Less

View Lastest Price from 3-Fluoro-5-bromoaniline manufacturers

Career Henan Chemical Co

Product: 3-Fluoro-5-bromoaniline 134168-97-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-09

134168-97-1, 3-Fluoro-5-bromoanilineRelated Search:

3-Fluoro-5-bromoaniline

5-BroMo-3-fluoroaniline

3-Bromo-5-fluoroaniline 97%

3-BroMo-5-fluoro-phenylaMine

Benzenamine, 3-bromo-5-fluoro-

3-Bromo-5-fluoroaniline,95%

3-Bromo-5-fluorobenzenamine

134168-97-1