3-Phenylpyridine-5-carboxaldehyde

Product Name: 3-Phenylpyridine-5-carboxaldehyde
CAS No.: 113118-84-6
Chemical Name: 3-Phenylpyridine-5-carboxaldehyde
Synonyms: 5-Phenylnicotinaldehyde;5-phenylpyridine-3-carbaldehyde;5-Phenyl-3-pyridinecarboxaldehyde;5-Phenylpyridine-3-carboxaldehyde;3-Phenylpyridine-5-carboxaldehyde;3-Pyridinecarboxaldehyde, 5-phenyl-
CBNumber: CB12506736
Molecular Formula: C12H9NO
Formula Weight: 183.21
MOL File: 113118-84-6.mol

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3-Phenylpyridine-5-carboxaldehyde Property

Boiling point:: 355.8±30.0 °C(Predicted)
Density: 1.147±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.05±0.20(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P399713
Product name: 5-Phenylnicotinaldehyde
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: P399713
Product name: 5-Phenylnicotinaldehyde
Packaging: 50mg
Price: $130
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0299057
Product name: 5-PHENYLPYRIDINE-3-CARBALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $497.68
Updated: 2021/12/16

Matrix Scientific

Product number: 191761
Product name: 3-Phenylpyridine-5-carboxaldehyde
Purity: 95%
Packaging: 5g
Price: $1650
Updated: 2021/12/16

Alichem

Product number: 113118846
Product name: 3-Phenylpyridine-5-carboxaldehyde
Packaging: 5g
Price: $3331.35
Updated: 2021/12/16

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3-Phenylpyridine-5-carboxaldehyde Chemical Properties,Usage,Production

Synthesis

113118-81-3

98-80-6

113118-84-6

General steps for the synthesis of 5-phenylpyridine-3-carbaldehyde: 1. reaction mixture preparation: 5-bromopyridine-3-carboxaldehyde (0.500 g, 2.69 mmol), tetrakis(triphenylphosphine)palladium (0.155 g, 0.134 mmol), and phenylboronic acid (0.492 g, 4.03 mmol) were dissolved in a biphasic mixture of degassed 2.0 M aqueous Na2CO3 solution (6.0 mL) and toluene (6.7 mL). 2. Reaction conditions: the mixture was heated to reflux for 2.5 hours. 3. Post-treatment: After completion of the reaction, the mixture was cooled to room temperature and diluted with water and ethyl acetate (EtOAc). The organic and aqueous layers were separated and the aqueous layer was extracted with ethyl acetate (1x). The organic layers were combined, washed with brine, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give an orange-brown oil (0.848 g). 4. Purification: 5-phenylpyridine-3-carbaldehyde (0.447 g, 91% yield) was purified by silica gel column chromatography as a light yellow solid. 5. Characterization: 1H NMR (500MHz, CDCl3) δ: 10.19 (s, 1H), 9.07 (s, 1H), 9.04 (s, 1H), 8.34 (s, 1H), 7.62 (d, J = 7.7Hz, 2H), 7.52 (t, J = 7.7Hz, 2H), 7.47-7.44 (m, 1H). Mass spectrum (MS): 184.2 (M + H)+; 216.2 (M + CH3OH + H)+.

References

[1] Patent: WO2007/70818, 2007, A1. Location in patent: Page/Page column 95
[2] Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012, vol. 67, # 1, p. 75 - 84
[3] Patent: US2014/296528, 2014, A1. Location in patent: Sheet 4

3-Phenylpyridine-5-carboxaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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113118-84-6, 3-Phenylpyridine-5-carboxaldehydeRelated Search:

3-Phenylpyridine-5-carboxaldehyde

5-phenylpyridine-3-carbaldehyde

5-Phenylnicotinaldehyde

5-Phenylpyridine-3-carboxaldehyde

5-Phenyl-3-pyridinecarboxaldehyde

3-Pyridinecarboxaldehyde, 5-phenyl-

113118-84-6