3-Biphenylboronic acid pinacol ester
- Product Name
- 3-Biphenylboronic acid pinacol ester
- CAS No.
- 912844-88-3
- Chemical Name
- 3-Biphenylboronic acid pinacol ester
- Synonyms
- 3-Biphenylboronic acid pinacol ester;Biphenyl-3-boronic Acid Pinacol Ester;[1,1'-Biphenyl]-3-boronic acid pinacol ester;1,1`-BIPHENYL]-3-YLBORONIC ACID PINACOL ESTER;3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl;-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;4,4,5,5-tetramethyl-2-(3-phenylphenyl)-1,3,2-dioxaborolane;1,3,2-Dioxaborolane,2-[1,1'-biphenyl]-3-yl-4,4,5,5-tetramethyl-;2-([1,1'-Biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- CBNumber
- CB12548101
- Molecular Formula
- C18H21BO2
- Formula Weight
- 280.17
- MOL File
- 912844-88-3.mol
3-Biphenylboronic acid pinacol ester Property
- Melting point:
- 82 °C
- Boiling point:
- 412.7±24.0 °C(Predicted)
- Density
- 1.05±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder to crystal
- color
- White to Almost white
- CAS DataBase Reference
- 912844-88-3
Safety
- HS Code
- 2931.90.6000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B6023
- Product name
- 2-([1,1'-Biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- Packaging
- 1G
- Price
- $37
- Updated
- 2025/07/31
- Product number
- B6023
- Product name
- 2-([1,1'-Biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- Packaging
- 5G
- Price
- $95
- Updated
- 2025/07/31
- Product number
- FB141393
- Product name
- 2-([1,1'-Biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- Packaging
- 500mg
- Price
- $140
- Updated
- 2021/12/16
- Product number
- CS-B1262
- Product name
- 1,3,2-Dioxaborolane,2-[1,1'-biphenyl]-3-yl-4,4,5,5-tetramethyl-
- Packaging
- 1g
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 40039
- Product name
- 2-([1,1'-Biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane,98%(GC)
- Purity
- 98%(GC)
- Packaging
- 1G
- Price
- $59.36
- Updated
- 2021/12/16
3-Biphenylboronic acid pinacol ester Chemical Properties,Usage,Production
Uses
suzuki reaction
Synthesis
2113-57-7
73183-34-3
912844-88-3
Synthesis Example 8: Synthesis of Intermediates I-8 3-Bromo-1,1 '-biphenyl (20 g, 85.8 mmol) was dissolved in dimethylformamide (DMF) (1 L) under nitrogen protection, and bis(pinacolato)diboron (26 g, 103 mmol), [1,1'-bis(diphenylphosphino)ferrocene]palladium(II) dichloride (0.7 g, 0.85 mmol), and potassium acetate (58 g 595 mmol). The reaction mixture was heated to 150 °C and refluxed for 5 hours. After completion of the reaction, water was added to the reaction solution, the mixture was filtered and dried in a vacuum oven. The resulting residue was separated and purified by fast column chromatography to afford the target compound I-8 (20 g, 85% yield). High resolution mass spectrometry (HRMS, 70 eV, EI+): the calculated m/z value for C18H21B2O was 280.1635 and the measured value was 280. Elemental analysis results: C, 77%; H, 7%.
References
[1] Patent: US2017/331067, 2017, A1. Location in patent: Paragraph 0212-0215
3-Biphenylboronic acid pinacol ester Preparation Products And Raw materials
Raw materials
Preparation Products
3-Biphenylboronic acid pinacol ester Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 3-Biphenylboronic acid pinacol ester manufacturers
- Product
- 3-Biphenylboronic acid pinacol ester 912844-88-3
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- G/KG/T
- Release date
- 2019-12-23