5-FLUORO-2-IODOBENZYL ALCOHOL

Product Name: 5-FLUORO-2-IODOBENZYL ALCOHOL
CAS No.: 877264-43-2
Chemical Name: 5-FLUORO-2-IODOBENZYL ALCOHOL
Synonyms: (5-Fluoro-2-iodophenyl);(5-fluoro-2-iodophenyl)methano;5-Fluoro-2-iodobenzylalcohol97%;(5-Fluoro-2-iodophenyl)Methanol;Benzenemethanol, 5-fluoro-2-iodo-;5-Fluoro-2-iodobenzyl alcohol 97%
CBNumber: CB12567317
Molecular Formula: C7H6FIO
Formula Weight: 252.02
MOL File: 877264-43-2.mol

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5-FLUORO-2-IODOBENZYL ALCOHOL Property

storage temp.: 2-8°C(protect from light)
Appearance: White to off-white Solid

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Safety

HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC48326
Product name: 5-Fluoro-2-iodobenzylalcohol
Purity: 97%
Packaging: 250mg
Price: $73
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2701-K-02
Product name: 5-Fluoro-2-iodobenzyl alcohol
Purity: 97%
Packaging: 250mg
Price: $80
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2701-K-02
Product name: 5-Fluoro-2-iodobenzyl alcohol
Purity: 97%
Packaging: 1g
Price: $240
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367394
Product name: (5-FLUORO-2-IODOPHENYL)METHANOL
Purity: 95.00%
Packaging: 5MG
Price: $496.72
Updated: 2021/12/16

Matrix Scientific

Product number: 119481
Product name: (5-Fluoro-2-iodophenyl)methanol
Purity: 95+%
Packaging: 1g
Price: $594
Updated: 2021/12/16

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5-FLUORO-2-IODOBENZYL ALCOHOL Chemical Properties,Usage,Production

Synthesis

52548-63-7

877264-43-2

Step 1: 5-fluoro-2-iodobenzoic acid (5.00 g, 18.80 mmol) was dissolved in tetrahydrofuran (50 mL) and cooled to 0 °C under nitrogen protection. The borane-dimethyl sulfide complex (3.57 mL, 37.60 mmol) was slowly added dropwise under stirring conditions, followed by gradual warming of the reaction mixture to room temperature. The reaction was stirred continuously for 16 hours at room temperature. Upon completion of the reaction, the mixture was carefully poured into ice and quenched by adding 10% aqueous potassium carbonate solution (50 mL). The mixture was extracted with dichloromethane (2 x 50 mL), the organic phases were combined, dried over magnesium sulfate and subsequently concentrated under reduced pressure to give 5-fluoro-2-iodobenzyl alcohol as a colorless solid (4.80 g, 91% yield).1H NMR (400 MHz, CDCl3): δ 7.68 (dd, 1H, J= Hz), 7.19 (dd, 1H, J= Hz), and 6.70 (td, 1H, J= Hz), 4.57 (d, 2H, J= Hz), 1.95 (t, 1H, J= Hz).

References

[1] Advanced Synthesis and Catalysis, 2015, vol. 357, # 14-15, p. 3206 - 3214
[2] Organic Letters, 2018, vol. 20, # 2, p. 345 - 348
[3] Patent: WO2013/132376, 2013, A1. Location in patent: Page/Page column 238
[4] Patent: US2006/52378, 2006, A1. Location in patent: Page/Page column 146
[5] Chemical Communications, 2013, vol. 49, # 31, p. 3254 - 3256

5-FLUORO-2-IODOBENZYL ALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

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5-FLUORO-2-IODOBENZYL ALCOHOL Suppliers

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877264-43-2, 5-FLUORO-2-IODOBENZYL ALCOHOLRelated Search:

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5-Fluoro-2-iodobenzyl alcohol 97%

(5-fluoro-2-iodophenyl)methano

5-Fluoro-2-iodobenzylalcohol97%

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877264-43-2