ChemicalBook > CAS DataBase List > 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester

3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester

Product Name
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
CAS No.
396731-40-1
Chemical Name
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
Synonyms
N-Boc-3,5-dioxopiperidine;5-dioxopiperidine-1-carboxylate;tert-Butyl 3,5-dioxopiperidine-1-carboxylat;tert-butyl 3,5-dioxo-1-piperidinecarboxylate;3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester;1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl e...;1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-diMethylethyl ester;3,5-dioxo-1-Piperidinecarboxylic acid 1,1-dimethylethyl ester (9CI ACI);1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl ester (9CI, ACI)
CBNumber
CB12618116
Molecular Formula
C10H15NO4
Formula Weight
213.23
MOL File
396731-40-1.mol
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3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Property

Boiling point:
346.2±32.0 °C(Predicted)
Density 
1.199±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
solid
pka
9.72±0.20(Predicted)
color 
Light yellow to yellow
CAS DataBase Reference
396731-40-1
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B694530
Product name
tert-Butyl3,5-dioxopiperidine-1-carboxylate
Packaging
100mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD71552
Product name
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
Packaging
500mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD71552
Product name
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
Packaging
1g
Price
$100
Updated
2021/12/16
AK Scientific
Product number
5216AB
Product name
tert-Butyl3,5-dioxopiperidine-1-carboxylate
Packaging
5g
Price
$134
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD71552
Product name
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
Packaging
2g
Price
$150
Updated
2021/12/16
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3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Chemical Properties,Usage,Production

Uses

3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


To a cooled (5 ??C) and stirred mixture of potassium 2-methyl-2-propoxide (29.7 g,0.27 mol) was added a solution of ethyl [A/-((1,1-dimethylethoxy)carbonyl),A/-(2-oxopropyl)]glycinate (65 g, 0.25 mol) in ethyl ether (200 ml) over a period of 1.5 h. The re- sulting mixture was stirred for an additional 3 h, and the formed precipitate was filtered offand washed with ethyl ether (2 x 100 ml). The solid was dissolved in water (150 ml), andacetic acid was added to adjust the pH to 4. The product was filtered, washed with water (2x 50 ml) and air dried to furnish 1 -[(1,1 -dimethylethoxy)carbonyl]-3,5-dioxopiperidine (28 g,52 %).>xxN'TOHPLC-MS: m/z: 158 (M+H-56).1H-NMR (DMSO-d6): 81.48 (9H, s), 4.03 (4H, s), 5.38 (1 H, s).

3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester manufacturers

Career Henan Chemical Co
Product
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester 396731-40-1
Price
US $1.00/KG
Min. Order
1G
Purity
98%
Supply Ability
100KG
Release date
2018-08-15

396731-40-1, 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylesterRelated Search:


  • 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
  • 1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-diMethylethyl ester
  • tert-Butyl 3,5-dioxopiperidine-1-carboxylat
  • 5-dioxopiperidine-1-carboxylate
  • N-Boc-3,5-dioxopiperidine
  • 1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl e...
  • 1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl ester (9CI, ACI)
  • 3,5-dioxo-1-Piperidinecarboxylic acid 1,1-dimethylethyl ester (9CI ACI)
  • tert-butyl 3,5-dioxo-1-piperidinecarboxylate
  • 396731-40-1