1-Chloroethyl (4-nitrophenyl) carbonate
- Product Name
- 1-Chloroethyl (4-nitrophenyl) carbonate
- CAS No.
- 101623-69-2
- Chemical Name
- 1-Chloroethyl (4-nitrophenyl) carbonate
- Synonyms
- 1-Chloroethyl 4-nitrophenyl carbonat;1-Chloroethyl p-nitrophenyl carbonate;1-Chloroethyl (4-nitrophenyl) carbonate;1-Chloroethyl-4-nitrophenyl carbonate (1-CENPC);Carbonic acid, 1-chloroethyl 4-nitrophenyl ester;Carbonic acid 1-chloro-ethyl ester 4-nitro-phenyl ester;Carbonic acid 4-nitro-phenyl ester 1-chloro-ethyl ester;Carbonic acid 4-nitro-phenyl ester 1-chloro-ethyl ester ISO 9001：2015 REACH
- CBNumber
- CB12629277
- Molecular Formula
- C9H8ClNO5
- Formula Weight
- 245.62
- MOL File
- 101623-69-2.mol
1-Chloroethyl (4-nitrophenyl) carbonate Property
- Melting point:
- 71.0-71.7 °C(Solv: hexane (110-54-3))
- Boiling point:
- 359.1±42.0 °C(Predicted)
- Density
- 1.415±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C984685
- Product name
- 1-Chloroethyl(4-Nitrophenyl)Carbonate
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 9801AL
- Product name
- 1-Chloroethyl(4-nitrophenyl)carbonate
- Packaging
- 10g
- Price
- $81
- Updated
- 2021/12/16
- Product number
- CS-M3307
- Product name
- 1-Chloroethyl4-nitrophenylcarbonate
- Packaging
- 10g
- Price
- $57
- Updated
- 2021/12/16
- Product number
- 9801AL
- Product name
- 1-Chloroethyl(4-nitrophenyl)carbonate
- Packaging
- 1g
- Price
- $14
- Updated
- 2021/12/16
- Product number
- CS-M3307
- Product name
- 1-Chloroethyl4-nitrophenylcarbonate
- Packaging
- 25g
- Price
- $112
- Updated
- 2021/12/16
1-Chloroethyl (4-nitrophenyl) carbonate Chemical Properties,Usage,Production
Uses
A clear, colourless to pale yellow liquid used as an intermediate in Gabapentin, an API.
Synthesis
To an ice cold reaction mixture containing p-nitrophenol (1.39 g, 10 mmol) and pyridine (0.81 g, 10 mmol) in dichloromethane (60 mL) was added 1-chloroethyl chloroformate (1.2 mL, 11 mmol). The mixture was stirred at 0° C for 30 min and then at room temperature for 1 hour. After removing the solvent under reduced pressure, the residue was dissolved in ether, washed with water, 10percent citric acid and water. The ether layer was dried over Na2SO4and evaporated under reduced pressure to give 2.4 g (97percent) of 1-Chloroethyl (4-nitrophenyl) carbonate as an off-white solid.
1-Chloroethyl (4-nitrophenyl) carbonate Preparation Products And Raw materials
Raw materials
Preparation Products
1-Chloroethyl (4-nitrophenyl) carbonate Suppliers
- Tel
- 732-484-9848
- Fax
- 888-484-5008
- sales@chemscene.com
- Country
- United States
- ProdList
- 3982
- Advantage
- 60
- Tel
- --
- Fax
- --
- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
- 58
View Lastest Price from 1-Chloroethyl (4-nitrophenyl) carbonate manufacturers
- Product
- 1-Chloroethyl (4-nitrophenyl) carbonate 101623-69-2
- Price
- US $101.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-28
- Product
- 1-chloroethyl (4-nitrophenyl) carbonate 101623-69-2
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 100 tons
- Release date
- 2020-01-10
- Product
- Carbonic acid 4-nitro-phenyl ester 1-chloro-ethyl ester 101623-69-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- ≥98%
- Supply Ability
- 200KG
- Release date
- 2019-08-30