α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-

Product Name: α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-
CAS No.: 131156-47-3
Chemical Name: α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-
Synonyms: 1,2:3,5-Di-O-isopropylidene-α-L-xylofuranose;(-)-1,2:3,5-di-O-isopropylidene-α-L-xylofuranose;1,2:3,5-DI-O-ISOPROPYLIDENE-ALPHA-L-XYLOFURANOSE;1,2:3,5-Bis-O-(1-methylethylidene)-α-L-xylofuranose;α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-;α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-;(1R,2S,6S,8S)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[6.4.0.02,6]dodecane;(3aS,3bR,7aS,8aS)-2,2,5,5-Tetramethyltetrahydro-7H-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine;(3aS,3bR,7aS,8aS)-2,2,5,5-tetramethyltetrahydro-3aH-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine
CBNumber: CB12666733
Molecular Formula: C11H18O5
Formula Weight: 230.26
MOL File: 131156-47-3.mol

More

Less

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)- Property

Melting point:: 39-40 °C
Boiling point:: 272.2±35.0 °C(Predicted)
Density: 1.112±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: MD10615
Product name: 1,2:3,5-Di-O-Isopropylidene-a-L-xylofuranose
Packaging: 5G
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: MD10615
Product name: 1,2:3,5-Di-O-Isopropylidene-a-L-xylofuranose
Packaging: 10g
Price: $125
Updated: 2021/12/16

AK Scientific

Product number: 8920CQ
Product name: (3As,3bR,7aS,8aS)-2,2,5,5-tetramethyltetrahydro-3aH-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine
Packaging: 250mg
Price: $203
Updated: 2021/12/16

Biosynth Carbosynth

Product number: MD10615
Product name: 1,2:3,5-Di-O-Isopropylidene-a-L-xylofuranose
Packaging: 25g
Price: $250
Updated: 2021/12/16

Biosynth Carbosynth

Product number: MD10615
Product name: 1,2:3,5-Di-O-Isopropylidene-a-L-xylofuranose
Packaging: 50g
Price: $400
Updated: 2021/12/16

More

Less

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)- Chemical Properties,Usage,Production

Synthesis

609-06-3

67-64-1

131156-47-3

Magnesium sulfate (160 g, 1.33 mol) and concentrated sulfuric acid (9.9 mL, 190 mmol) were added to a solution of (2S,3R,4S)-2,3,4,5-tetrahydroxyvaleraldehyde (99.0 g, 659 mmol) in acetone (1.2 L) at room temperature. The reaction mixture was stirred for 12 hours. After completion of the reaction, filtration was carried out and the filter cake was washed with acetone (300 mL x 2). The filtrates were combined and the pH was adjusted to 7 with 25% ammonia, at which point a solid precipitated and filtered again. The solids were washed with acetone (150 mL x 2). All the filtrates were combined and concentrated under reduced pressure to afford the target product (3aS,3bR,7aS,8aS)-2,2,5,5-tetramethyltetrahydro-3aH-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxolane (Ib) as a yellow oil (128.0 g, 84.3% yield).

References

[1] Patent: CN106892948, 2017, A. Location in patent: Paragraph 0183; 0185; 0186; 0187
[2] Nucleosides, Nucleotides and Nucleic Acids, 2001, vol. 20, # 4-7, p. 703 - 706
[3] Collection of Czechoslovak Chemical Communications, 2006, vol. 71, # 7, p. 1063 - 1087
[4] Patent: WO2012/140596, 2012, A1. Location in patent: Page/Page column 53-55

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)- Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)- Suppliers

China 25 India 1 United Kingdom 1 United States 2 Global 29

skychemical Co.Ltd

Tel: 021-20958197 20965099
Fax: 021-20960837
Email: sales@skychemical.com
Country: China
ProdList: 1183
Advantage: 57

ShangHai Caerulum Pharma Discovery Co., Ltd.

Tel: 18149758185
Email: sales-cpd@caerulumpharma.com
Country: China
ProdList: 3506
Advantage: 58

skychemical Co.Ltd

Tel: 021-20960837,QQ1332204249
Fax: 021-20960837
Email: sales@skychemical.com
Country: China
ProdList: 3341
Advantage: 55

ChengDu TongChuangYuan Pharmaceutical Co.Ltd

Tel: 028-83379370 13880556291
Fax: 028-87747383
Email: tcy@tcypharm.com
Country: China
ProdList: 7218
Advantage: 58

Jinan elephant international trading co., LTD

Tel
Fax: -
Email: 13006575422@163.com
Country: China
ProdList: 6355
Advantage: 58

Dezhou LonWel Pharmaceutical Technology Co., Ltd.

Tel: 13761310616
Fax: QQ: 39324283
Email: 39324283@qq.com
Country: China
ProdList: 1643
Advantage: 58

Jinan Samuel Pharmaceutical Co., Ltd.

Tel: 0531-88821801 15192360884
Fax: 0531-88821802
Email: 605818151@qq.com
Country: China
ProdList: 417
Advantage: 58

Aikon International Limited

Tel: 025-66113011 13155353615
Fax: (7)02557626880
Email: qzhang@aikonchem.com
Country: China
ProdList: 15394
Advantage: 58

Jinan Yaoyan Pharmaceutical Co., Ltd.

Tel
Fax: -
Email: jnyaoyan@163.com
Country: China
ProdList: 3069
Advantage: 58

Shanghai Moss Medicine Technology Co., Ltd.

Tel: +86-188369842 +86-15618151133
Fax: QQ188369842
Email: 188369842@qq.com
Country: China
ProdList: 1959
Advantage: 58

131156-47-3, α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-Related Search:

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-

1,2:3,5-DI-O-ISOPROPYLIDENE-ALPHA-L-XYLOFURANOSE

(-)-1,2:3,5-di-O-isopropylidene-α-L-xylofuranose

(3aS,3bR,7aS,8aS)-2,2,5,5-tetramethyltetrahydro-3aH-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine

(1R,2S,6S,8S)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[6.4.0.02,6]dodecane

(3aS,3bR,7aS,8aS)-2,2,5,5-Tetramethyltetrahydro-7H-[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine

1,2:3,5-Bis-O-(1-methylethylidene)-α-L-xylofuranose

1,2:3,5-Di-O-isopropylidene-α-L-xylofuranose

α-L-Xylofuranose,1,2:3,5-bis-O-(1-Methylethylidene)-

131156-47-3