4-Bromo-2-iodobenzaldehyde

Product Name: 4-Bromo-2-iodobenzaldehyde
CAS No.: 1261470-87-4
Chemical Name: 4-Bromo-2-iodobenzaldehyde
Synonyms: 4-Bromo-2-iodobenzaldehyde;2-IODO-4-BROMO BENZALDEHYDE;Benzaldehyde, 4-bromo-2-iodo-;4-Bromo-2-iodobenzaldehyde97%;4-Bromo-2-iodobenzaldehyde 97%
CBNumber: CB12696505
Molecular Formula: C7H4BrIO
Formula Weight: 310.91
MOL File: 1261470-87-4.mol

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4-Bromo-2-iodobenzaldehyde Property

Boiling point:: 323.2±37.0 °C(Predicted)
Density: 2.231±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: powder
color: Off white to faint cream
InChI: InChI=1S/C7H4BrIO/c8-6-2-1-5(4-10)7(9)3-6/h1-4H
InChIKey: JFFYPBIPKMTEEQ-UHFFFAOYSA-N
SMILES: C(=O)C1=CC=C(Br)C=C1I

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Safety

HS Code: 2913000090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B681413
Product name: 4-Bromo-2-Iodobenzaldehyde
Packaging: 100mg
Price: $90
Updated: 2021/12/16

TRC

Product number: B681413
Product name: 4-Bromo-2-Iodobenzaldehyde
Packaging: 50mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B681413
Product name: 4-Bromo-2-Iodobenzaldehyde
Packaging: 500mg
Price: $330
Updated: 2021/12/16

AK Scientific

Product number: 2692AJ
Product name: 4-Bromo-2-iodobenzaldehyde
Packaging: 5g
Price: $995
Updated: 2021/12/16

Apolloscientific

Product number: OR40677
Product name: 4-Bromo-2-iodobenzaldehyde
Purity: 97%
Packaging: 5g
Price: $743
Updated: 2021/12/16

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4-Bromo-2-iodobenzaldehyde Chemical Properties,Usage,Production

Synthesis

885681-96-9

1261470-87-4

General procedure for the synthesis of 4-bromo-2-iodobenzaldehyde (17b) from 4-bromo-1-(bromomethyl)-2-iodobenzene: A solution of N-methylmorpholine-N-oxide (2.81 g, 23.2 mmol) and 4A molecular sieves (19 g) in acetonitrile (60 mL) was added to a dry 250 mL Schlenk flask under nitrogen protection and cooled to 0 °C. This was followed by rapid addition of benzyl bromide 15b (2.9 g, 7.7 mmol). The reaction mixture was kept at 0 °C for 2 h and then slowly warmed up to room temperature. Upon completion of the reaction, it was filtered through a short column of silica gel (SiO2:hexane) to afford the off-white solid product 17b (2.15 g, 6.92 mmol, 90% yield). The product was characterized as follows: 1H-NMR (400 MHz, CDCl3) δ: 9.99 (s, 1H), 8.13 (d, 1H, J = 0.8 Hz), 7.73 (dd, 1H, J = 8.3, 0.8 Hz), 7.61 (dd, 1H, J = 8.3, 0.8 Hz); 13C-NMR (100 MHz, CDCl3) δ: 194.7, 142.8, 134.1, 132.3, 131.1, 130.2, 100.9; HRMS (EI) m/z calculated value of C7H4BrIO [M?]+: 309.8490, measured value: 309.8489.

References

[1] Journal of Organic Chemistry, 2011, vol. 76, # 7, p. 2227 - 2239
[2] Synthesis, 2011, # 15, p. 2387 - 2391
[3] Patent: WO2011/127383, 2011, A2. Location in patent: Page/Page column 75

4-Bromo-2-iodobenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Bromo-2-iodobenzaldehyde Suppliers

China 49 India 2 United Kingdom 1 United States 4 Global 56

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View Lastest Price from 4-Bromo-2-iodobenzaldehyde manufacturers

Career Henan Chemical Co

Product: 4-Bromo-2-iodobenzaldehyde 1261470-87-4
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200g
Release date: 2020-02-01

1261470-87-4, 4-Bromo-2-iodobenzaldehydeRelated Search:

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4-Bromo-2-iodobenzaldehyde

4-Bromo-2-iodobenzaldehyde97%

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4-Bromo-2-iodobenzaldehyde 97%

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1261470-87-4