2-formyl-1H-Indole-5-carboxylic acid methyl ester
- Product Name
- 2-formyl-1H-Indole-5-carboxylic acid methyl ester
- CAS No.
- 880360-85-0
- Chemical Name
- 2-formyl-1H-Indole-5-carboxylic acid methyl ester
- Synonyms
- methyl 2-formyl-1H-indole-5-carboxylate;2-formyl-1H-Indole-5-carboxylic acid methyl ester;1H-Indole-5-carboxylic acid, 2-formyl-, methyl ester
- CBNumber
- CB12756188
- Molecular Formula
- C11H9NO3
- Formula Weight
- 203.19
- MOL File
- 880360-85-0.mol
2-formyl-1H-Indole-5-carboxylic acid methyl ester Property
- Boiling point:
- 404.4±25.0 °C(Predicted)
- Density
- 1.341±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 14.14±0.30(Predicted)
- Appearance
- Light yellow to yellow Solid
N-Bromosuccinimide Price
- Product number
- CS-0062133
- Product name
- Methyl2-formyl-1H-indole-5-carboxylate
- Packaging
- 250mg
- Price
- $260
- Updated
- 2021/12/16
- Product number
- 2767AQ
- Product name
- 2-Formyl-1H-indole-5-carboxylicacidmethylester
- Packaging
- 250mg
- Price
- $689.6
- Updated
- 2021/12/16
- Product number
- CS-0062133
- Product name
- Methyl2-formyl-1H-indole-5-carboxylate
- Packaging
- 5g
- Price
- $4395
- Updated
- 2021/12/16
- Product number
- H2346
- Product name
- 2-formyl-1H-Indole-5-carboxylicacidmethylester
- Purity
- 97.00%
- Packaging
- 25G
- Price
- $7320
- Updated
- 2021/12/16
- Product number
- A222533
- Product name
- Methyl2-formyl-1H-indole-5-carboxylate
- Purity
- 97%
- Packaging
- 100mg
- Price
- $166
- Updated
- 2021/12/16
2-formyl-1H-Indole-5-carboxylic acid methyl ester Chemical Properties,Usage,Production
Synthesis
190071-26-2
880360-85-0
General procedure for the synthesis of methyl 2-(hydroxymethyl)-1H-indole-5-carboxylate from methyl 2-(hydroxymethyl)-1H-indole-5-carboxylate: to a stirred solution of methyl 2-(hydroxymethyl)-1H-indole-5-carboxylate (4.7 g, 23.1 mmol) in 70 mL of chloroform was added MnO2 (12.5 g, 115.4 mmol) in batches. After 14 hours of reaction, the mixture was filtered through a diatomaceous earth plug and the filtrate was concentrated under reduced pressure to give methyl 2-formyl-1H-indole-5-carboxylate (4.0 g, 85% yield) as a brown oil. The product could be used in subsequent reactions without further purification. Thin layer chromatography (TLC) Rf = 0.21 (20% EtOAc/hexane). Elemental analysis (C11H11NO3) Calculated value: exact mass 203.06; measured value: 203.06. low resolution mass spectrometry (LRMS) APCI (M-1) m/z 202.
References
[1] Patent: US2006/69087, 2006, A1. Location in patent: Page/Page column 14
2-formyl-1H-Indole-5-carboxylic acid methyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
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