2-FLUORO-3-IODOBENZOIC ACID

Product Name: 2-FLUORO-3-IODOBENZOIC ACID
CAS No.: 447464-03-1
Chemical Name: 2-FLUORO-3-IODOBENZOIC ACID
Synonyms: BUTTPARK 122\01-03;2-FLUORO-3-IODOBENZOIC ACID;Benzoic acid, 2-fluoro-3-iodo-
CBNumber: CB1288030
Molecular Formula: C7H4FIO2
Formula Weight: 266.01
MOL File: Mol file

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2-FLUORO-3-IODOBENZOIC ACID Property

Boiling point:: 331.0±27.0 °C(Predicted)
Density: 2.074±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 2.92±0.10(Predicted)
form: crystalline powder
color: Faint brown

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Safety

Hazard Codes: T
Risk Statements: 25
Safety Statements: 45
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B435038
Product name: 2-Fluoro-3-iodobenzoicAcid
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: PC32730
Product name: 2-Fluoro-3-iodobenzoicacid
Packaging: 1g
Price: $44
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2621-K-07
Product name: 2-Fluoro-3-iodobenzoic acid
Packaging: 1g
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: PC32730
Product name: 2-Fluoro-3-iodobenzoicacid
Packaging: 5g
Price: $160
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0063219
Product name: 2-FLUORO-3-IODOBENZOIC ACID
Purity: 95.00%
Packaging: 250MG
Price: $415
Updated: 2021/12/16

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2-FLUORO-3-IODOBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

211943-27-0

447464-03-1

General procedure for the synthesis of 2-fluoro-3-iodobenzoic acid from 2-fluoro-3-iodobenzonitrile: A mixture of 2-fluoro-3-iodobenzonitrile (5.00 g, 20.2 mmol), dioxane (16 mL), and concentrated sulfuric acid (25 mL) was heated to 115 °C and reacted for 4 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble material. Water was added to the filtrate and the aqueous phase was extracted with ethyl acetate. The organic layers were combined, dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give 2-fluoro-3-iodobenzoic acid (4.42 g, 82% yield) as a white solid. Mass spectrum (LRMS) m/z: 265 ([M-H]-). 1H-NMR (CDCl3) δ: 6.94-7.01 (m, 1H), 7.90-7.97 (m, 2H).

References

[1] Patent: EP2113503, 2009, A1. Location in patent: Page/Page column 32
[2] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 21, p. 6253 - 6257

2-FLUORO-3-IODOBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-FLUORO-3-IODOBENZOIC ACID Suppliers

China 83 India 2 United Kingdom 2 United States 10 Global 97

PharmaBlock Sciences (Nanjing),Inc.

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View Lastest Price from 2-FLUORO-3-IODOBENZOIC ACID manufacturers

Career Henan Chemical Co

Product: 2-FLUORO-3-IODOBENZOIC ACID 447464-03-1
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2020-02-17

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