3-ethylbicyclo[3.2.0]hept-3-en-6-one
- Product Name
- 3-ethylbicyclo[3.2.0]hept-3-en-6-one
- CAS No.
- 1235479-59-0
- Chemical Name
- 3-ethylbicyclo[3.2.0]hept-3-en-6-one
- Synonyms
- 3-ethylbicyclo[3.2.0]hept-3-en-6-one;3-Ethylbicyclo[3.2.0]hept-3-ene-6-one;Bicyclo[3.2.0]hept-3-en-6-one, 3-ethyl-;3-ethylbicyclic [3.2.0] hept-3-ene-6-ketone
- CBNumber
- CB13051615
- Molecular Formula
- C9H12O
- Formula Weight
- 136.19
- MOL File
- 1235479-59-0.mol
3-ethylbicyclo[3.2.0]hept-3-en-6-one Property
- Boiling point:
- 212.5±9.0 °C(Predicted)
- Density
- 1.043±0.06 g/cm3(Predicted)
N-Bromosuccinimide Price
- Product number
- CM325605
- Product name
- 3-ethylbicyclo[3.2.0]hept-3-en-6-one
- Purity
- 95%+
- Packaging
- 1000g
- Price
- $4000
- Updated
- 2021/12/16
3-ethylbicyclo[3.2.0]hept-3-en-6-one Chemical Properties,Usage,Production
Uses
3-ethylbicyclo[3.2.0]hept-3-en-6-one is an important organic compound mainly used in chemical research. Currently, it is mainly used to study the separation of its enantiomers.
Synthesis
3-ethylbicyclo[3.2.0]hept-3-en-6-one was synthesised from 4-Ethyl-3-hydroxyhept-6-enoic acid.
Preparation method: Intermediate (39.0 g, 226 mmol), acetic anhydride (195 mL), potassium acetate (51.4 g, 542 mmol) were added to the reaction flask, and the reaction was stirred at room temperature for 1 h, and the temperature was raised to 130 °C,The reaction was stirred for 4h, and the reaction was completed by GC monitoring. Add H2O (200mL), extract with EA (200mL*3), wash with 1N NaOH (100mL) and water (200mL), dry over anhydrous Na2SO4, filter, spin-dried to obtain the crude product of 3-ethylbicyclo[3.2.0]hept-3-en-6-one, and distilled under high vacuum to obtain 16g of 3-ethylbicyclo[3.2.0]hept-3-en-6-one , the appearance is colorless to light yellow oily liquid, the yield is 51.6%.
3-ethylbicyclo[3.2.0]hept-3-en-6-one Preparation Products And Raw materials
Raw materials
Preparation Products
3-ethylbicyclo[3.2.0]hept-3-en-6-one Suppliers
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- Product
- 3-Ethylbicyclo[3.2.0]hept-3-en-6-one 1235479-59-0
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 500kg
- Release date
- 2023-04-04
- Product
- 3-ethylbicyclo[3.2.0]hept-3-en-6-one 1235479-59-0
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-08