2-FLUORO-3-PYRIDINEMETHANAMINE
Application- Product Name
- 2-FLUORO-3-PYRIDINEMETHANAMINE
- CAS No.
- 859164-64-0
- Chemical Name
- 2-FLUORO-3-PYRIDINEMETHANAMINE
- Synonyms
- RARECHEM AL BW 2476;2-FLUORO-3-PYRIDINEMETHANAMINE;(2-fluoro-3-pyridyl)methanamine;(2-FLUOROPYRIDIN-3-YL)METHANAMINE;(2-FLUOROPYRIDIN-3-YL)METHANAMINE HCL;2-Fluoro-3-pyridinemethanamine,hydrochloride;2-Fluoropyridine-3-methanamine Hydrochloride;(2-fluoro-3-pyridyl)methanamine hydrochloride;2-fluoro-3-pyridineMethanaMine dihydrochloride;2-fluoro-3-(aminomethyl)pyridine hydrochloride
- CBNumber
- CB1372832
- Molecular Formula
- C6H7FN2
- Formula Weight
- 126.13
- MOL File
- 859164-64-0.mol
2-FLUORO-3-PYRIDINEMETHANAMINE Property
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- F600108
- Product name
- (2-Fluoropyridin-3-yl)methanaminehydrochloride
- Packaging
- 100mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- HCH0068900
- Product name
- 2-FLUORO-3-PYRIDINEMETHANAMINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $933.24
- Updated
- 2021/12/16
- Product number
- HCH0068900
- Product name
- 2-FLUORO-3-PYRIDINEMETHANAMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1346.73
- Updated
- 2021/12/16
- Product number
- 3392AC
- Product name
- (2-Fluoropyridin-3-yl)methanaminehydrochloride
- Packaging
- 25g
- Price
- $1967
- Updated
- 2021/12/16
- Product number
- HCH0068900
- Product name
- 2-FLUORO-3-PYRIDINEMETHANAMINE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $2674.98
- Updated
- 2021/12/16
2-FLUORO-3-PYRIDINEMETHANAMINE Chemical Properties,Usage,Production
Application
2-Fluoro-3-pyridinemethylmethylamine is an amine organic compound that can be used as a pharmaceutical synthesis intermediate.
Synthesis
3939-13-7
859164-64-0
General procedure for the synthesis of 2-fluoro-3-pyridinylmethylamine from 2-fluoro-3-cyanopyridine: first, C-(2-fluoro-pyridin-3-yl)-methylamine hydrochloride was prepared. Concentrated hydrochloric acid (0.46 mL) was slowly added to a suspension of methanol (10 mL) containing 2-fluoro-3-cyanopyridine (0.34 g, 2.8 mmol) and 5% Pd/C (0.5 g) at room temperature. Subsequently, the reaction suspension was stirred continuously for 6 hours under a hydrogen atmosphere at 1 atmosphere. Upon completion of the reaction, the reaction mixture was filtered and the filtrate concentrated. Ether was added to the concentrated residue and HCl gas was passed through the suspension bulge. The resulting precipitate was filtered and dried to give the target product 2-fluoro-3-pyridylmethylmethylamine (0.37 g, 82% yield). Substance spectral analysis (ES) of the product showed a m/z of 127.1 ([M + H]+). The NMR hydrogen spectrum (400 MHz, DMSO-d6) data were as follows: δ 8.65 (broad single peak, 3H), 8.24 (multiple peaks, 1H), 8.16 (multiple peaks, 1H), 7.41 (multiple peaks, 1H), 4.06 (multiple peaks, 2H).
References
[1] Patent: WO2005/66126, 2005, A1. Location in patent: Page/Page column 59
2-FLUORO-3-PYRIDINEMETHANAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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