ETHYL 3-CHLOROBENZOYLFORMATE

Product Name: ETHYL 3-CHLOROBENZOYLFORMATE
CAS No.: 62123-73-3
Chemical Name: ETHYL 3-CHLOROBENZOYLFORMATE
Synonyms: ETHYL 3-CHLOROBENZOYLFORMATE;Ethyl 2-(3-chlorophenyl)-2-oxoacetate;(3-Chlorophenyl)oxoacetic acid ethyl ester;(3-CHLOROPHENYL)GLYOXYLIC ACID ETHYL ESTER;3-Chloro-oxo-benzeneacetic acid ethyl ester;Benzeneacetic acid,3-chloro-a-oxo-, ethyl ester;Benzeneacetic acid, 3-chloro-α-oxo-, ethyl ester
CBNumber: CB1419685
Molecular Formula: C10H9ClO3
Formula Weight: 212.63
MOL File: 62123-73-3.mol

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ETHYL 3-CHLOROBENZOYLFORMATE Property

Boiling point:: 88°C 0,1mm
Density: 1.2270 g/cm3
storage temp.: Sealed in dry,Room Temperature
Appearance: pale yellow liquid
CAS DataBase Reference: 62123-73-3(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Oakwood

Product number: 023000
Product name: Ethyl3-chlorobenzoylformate
Purity: 96%
Packaging: 250mg
Price: $125
Updated: 2021/12/16

Oakwood

Product number: 023000
Product name: Ethyl3-chlorobenzoylformate
Purity: 96%
Packaging: 1g
Price: $250
Updated: 2021/12/16

Matrix Scientific

Product number: 086335
Product name: Ethyl 3-chlorobenzoylformate
Purity: 97%
Packaging: 1g
Price: $252
Updated: 2021/12/16

Rieke Metals

Product number: KE0100
Product name: (3-Chlorophenyl)oxoaceticacidethylester
Packaging: 1g
Price: $364
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0026010
Product name: ETHYL 3-CHLOROBENZOYLFORMATE
Purity: 95.00%
Packaging: 5G
Price: $670
Updated: 2021/12/16

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ETHYL 3-CHLOROBENZOYLFORMATE Chemical Properties,Usage,Production

Synthesis

64-17-5

21667-62-9

62123-73-3

GENERAL METHODS: 3-Chlorobenzoylacetonitrile (1.0 mmol) and PIDA (2.2 mmol) were dissolved in ethanol (8 mL), and the reaction was stirred under reflux conditions for 0.5 hours. The reaction process was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent ratio 20:1 petroleum ether/ethyl acetate) to afford the target product ethyl 3-chlorobenzoylformate. Note: The solvent used in this synthesis step is methanol (MeOH).

References

[1] Tetrahedron Letters, 2015, vol. 56, # 24, p. 3793 - 3795

ETHYL 3-CHLOROBENZOYLFORMATE Preparation Products And Raw materials

Raw materials

Preparation Products

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ETHYL 3-CHLOROBENZOYLFORMATE Suppliers

China 39 Germany 3 United Kingdom 6 United States 11 Global 59

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62123-73-3, ETHYL 3-CHLOROBENZOYLFORMATERelated Search:

ETHYL 2-CHLOROBENZOYLFORMATE ETHYL 4-CHLOROBENZOYLFORMATE,Ethyl 4-chlorobenzoylformate Ethyl 2-(2,4-dichlorophenyl)-2-oxoacetate (4-Chlorophenyl)glyoxylic acid ethyl ester ETHYL 3,5-DICHLOROBENZOYLFORMATE ETHYL 3-CHLORO-4-FLUOROBENZOYLFORMATE ETHYL 2,3-DICHLOROBENZOYLFORMATE ETHYL 3,4-DICHLOROBENZOYLFORMATE ETHYL 3-CHLOROBENZOYLFORMATE ETHYL 3-CHLORO-5-FLUOROBENZOYLFORMATE

(3-CHLOROPHENYL)GLYOXYLIC ACID ETHYL ESTER

ETHYL 3-CHLOROBENZOYLFORMATE

(3-Chlorophenyl)oxoacetic acid ethyl ester

Ethyl 2-(3-chlorophenyl)-2-oxoacetate

3-Chloro-oxo-benzeneacetic acid ethyl ester

Benzeneacetic acid,3-chloro-a-oxo-, ethyl ester

Benzeneacetic acid, 3-chloro-α-oxo-, ethyl ester

62123-73-3

Aromatic Esters