ChemicalBook > CAS DataBase List > 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE

2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE

Product Name: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE
CAS No.: 808-57-1
Chemical Name: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE
Synonyms: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE;Triphenylene, 2,3,6,7,10,11-hexamethoxy-;2,3,6,7,10,11-Hexamethoxytriphenylene>2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE, 9 9%
CBNumber: CB1435481
Molecular Formula: C24H24O6
Formula Weight: 408.44
MOL File: 808-57-1.mol

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2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE Property

Melting point:: 310-317℃
Boiling point:: 578.6±45.0 °C(Predicted)
Density: 1.216
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
color: Purple to Dark purple to Dark red
InChI: InChI=1S/C24H24O6/c1-25-19-7-13-14(8-20(19)26-2)16-10-22(28-4)24(30-6)12-18(16)17-11-23(29-5)21(27-3)9-15(13)17/h7-12H,1-6H3
InChIKey: TXROZCSFVVIBFI-UHFFFAOYSA-N
SMILES: C1=C2C(C3C(C4C2=CC(OC)=C(OC)C=4)=CC(OC)=C(OC)C=3)=CC(OC)=C1OC
CAS DataBase Reference: 808-57-1

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Safety

Safety Statements: 24/25
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: T341509
Product name: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $185
Updated: 2025/07/31

Sigma-Aldrich

Product number: T341509
Product name: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE
Purity: Aldrich
Packaging: 250mg
Price: $179
Updated: 2024/03/01

TCI Chemical

Product number: H0898
Product name: 2,3,6,7,10,11-Hexamethoxytriphenylene
Purity: >95.0%(GC)
Packaging: 1g
Price: $145
Updated: 2025/07/31

TCI Chemical

Product number: H0898
Product name: 2,3,6,7,10,11-Hexamethoxytriphenylene
Purity: >95.0%(GC)
Packaging: 5g
Price: $436
Updated: 2025/07/31

TRC

Product number: H296713
Product name: 2,3,6,7,10,11-Hexamethoxytriphenylene
Packaging: 10mg
Price: $45
Updated: 2021/12/16

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2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE Chemical Properties,Usage,Production

Uses

2,3,6,7,10,11-Hexamethoxytriphenylene is a useful research chemical used in the preparation and synthesis of triphenylene-??based discotic mesogens.

Synthesis

91-16-7

808-57-1

The general procedure for the synthesis of 2,3,6,7,10,11-hexamethoxytriphenylene from o-anisidine is as follows: B-type crystals of 2,3,6,7,10,11-hexahydroxytriphenylene monohydrate were first synthesized with reference to the methods reported in Synthesis, 477, 1994 and JP-A-8-119894. This was done as follows: 1,2-dimethoxybenzene (31.78 g, 0.23 mol) was co-dissolved with anhydrous ferric chloride (120 g, 0.74 mol) in 70% sulfuric acid and the reaction was stirred at 25 °C for 24 hours. After completion of the reaction, the reaction mixture was slowly poured into ice water (500 g) and the precipitated crystals were collected by filtration. Subsequently, the resulting crystals were washed with distilled water (1 L) and dried to give light purple 2,3,6,7,10,11-hexamethoxytriphenylene (28.2 g, 90.1% yield as 1,2-dimethoxybenzene). This method is derived from Synthesis, 477, 1994.

References

[1] Angewandte Chemie - International Edition, 2010, vol. 49, # 44, p. 8209 - 8213
[2] Synthesis, 1994, vol. 1, # 5, p. 477 - 478
[3] Patent: EP2177495, 2010, A1. Location in patent: Page/Page column 12
[4] Synthetic Communications, 1999, vol. 29, # 10, p. 1767 - 1771
[5] Journal of the American Chemical Society, 2017, vol. 139, # 46, p. 16759 - 16767

2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE 808-57-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-10-14

Career Henan Chemical Co

Product: 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE 808-57-1
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 100KG
Release date: 2018-12-21

808-57-1, 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENERelated Search:

Uracil 3-METHOXYPHENANTHRENE 2,3,6,7,10,11-Triphenylenehexol 2-Methoxyphenanthrene 3-HYDROXY-PHENANTHRENE Triphenylene 2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE 2 3-DIMETHOXYNAPHTHALENE 97 2,3-Dihydroxynaphthalene 2,3,6,7,10,11-HEXAACETOXYTRIPHENYLENE 2-HYDROXY-PHENANTHRENE 2,3,6,7,10,11-HEXAKIS(PENTYLOXY)TRIPHENYLENE

2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE

2,3,6,7,10,11-HEXAMETHOXYTRIPHENYLENE, 9 9%

2,3,6,7,10,11-Hexamethoxytriphenylene&gt

Triphenylene, 2,3,6,7,10,11-hexamethoxy-

808-57-1

C24H24O6

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