9-ACETYLCARBAZOLE 97
- Product Name
- 9-ACETYLCARBAZOLE 97
- CAS No.
- 574-39-0
- Chemical Name
- 9-ACETYLCARBAZOLE 97
- Synonyms
- NSC 39028;JACS-574-39-0;9-ACETYLCARBAZOLE 97;1-(9H-Carbazol-9-yl)ethanone;Ethanone, 1-(9H-carbazol-9-yl)-
- CBNumber
- CB1498864
- Molecular Formula
- C14H11NO
- Formula Weight
- 209.24
- MOL File
- 574-39-0.mol
9-ACETYLCARBAZOLE 97 Property
- Melting point:
- 77-79 °C (lit.)
- Boiling point:
- 348.61°C (rough estimate)
- Density
- 1.1580
- refractive index
- 1.6400 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Almost white
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-36/37/38
- Safety Statements
- 26-36
- WGK Germany
- 3
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 649201
- Product name
- 9-Acetylcarbazole
- Purity
- 97%
- Packaging
- 1g
- Price
- $59
- Updated
- 2023/06/20
- Product number
- A3373
- Product name
- 9-Acetylcarbazole
- Packaging
- 1G
- Price
- $48
- Updated
- 2025/07/31
- Product number
- A3373
- Product name
- 9-Acetylcarbazole
- Packaging
- 5G
- Price
- $140
- Updated
- 2025/07/31
- Product number
- A172008
- Product name
- 9-Acetylcarbazole
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 6174AF
- Product name
- 9-Acetylcarbazole
- Packaging
- 250mg
- Price
- $147
- Updated
- 2021/12/16
9-ACETYLCARBAZOLE 97 Chemical Properties,Usage,Production
Synthesis
108-05-4
86-74-8
574-39-0
Vinyl acetate (1a, 167 mg, 1 mmol) and carbazole (2, 430 mg, 5 mmol) were mixed with [Ir(Cl)(cod)]2 (6.7 mg, 0.01 mmol), Na2CO3 (127 mg, 1.2 mmol) and toluene (1 mL) under argon protection and the reaction was stirred for 15 h at 100 °C. The reaction was carried out by GC analysis. The conversion and yield of the product were calculated by gas chromatography (GC) analysis with internal standard method, and the yield of 1-(9H-carbazol-9-yl)ethanone (3a) was obtained as 96%. Product 3a was purified by column chromatography (using 230-400 mesh silica gel with hexane containing 5% Et3N as eluent) in a final yield of 94% (181 mg). For product 3e, the separation was carried out by column chromatography only (using 70-230 mesh alumina and hexane as eluent).
References
[1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983, vol. 19, # 11, p. 1192 - 1197
[2] Khimiya Geterotsiklicheskikh Soedinenii, 1983, # 11, p. 1504 - 1509
[3] Synlett, 2017, vol. 28, # 6, p. 719 - 723
9-ACETYLCARBAZOLE 97 Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-ACETYLCARBAZOLE 97 manufacturers
- Product
- 1-(9H-Carbazol-9-yl)ethanone 574-39-0
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-20
- Product
- 9-ACETYLCARBAZOLE 97 574-39-0
- Price
- US $30.00-28.00/Kg
- Min. Order
- 1Kg
- Purity
- 99.0% up
- Supply Ability
- 50 tons per month
- Release date
- 2022-09-29
- Product
- 9-ACETYLCARBAZOLE 97 574-39-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98$
- Supply Ability
- 200kg
- Release date
- 2019-08-30