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ALPHA-BROMOISOBUTYRIC ACID

Product Name
ALPHA-BROMOISOBUTYRIC ACID
CAS No.
55-52-7
Chemical Name
ALPHA-BROMOISOBUTYRIC ACID
Synonyms
JB-516;Phenizine;Pheniprazine;PHENYLISOPROPYLHYDRAZINE;2-HYDRAZINOPROPYLBENZENE;1-phenylpropan-2-ylhydrazine;BETA-PHENYLISOPROPYLHYDRAZINE;(1-Methyl-2-phenylethyl)hydrazine;HYDRAZINE,(ALPHA-METHYLPHENETHYL)-;Hydrazine, (1-methyl-2-phenylethyl)-
CBNumber
CB1547184
Molecular Formula
C9H14N2
Formula Weight
150.22
MOL File
55-52-7.mol
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ALPHA-BROMOISOBUTYRIC ACID Property

Melting point:
25°C
Boiling point:
261.79°C (rough estimate)
Density 
0.9372 (rough estimate)
refractive index 
1.6210 (estimate)
pka
8.00±0.70(Predicted)
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Safety

Toxicity
LD50 orl-rat: 34 mg/kg 27ZQAG -,353,72
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0099226
Product name
1-(1-PHENYLPROPAN-2-YL)HYDRAZINE
Purity
95.00%
Packaging
5MG
Price
$503.66
Updated
2021/12/16
Labseeker
Product number
SC-39255
Product name
1-(1-phenylpropan-2-yl)hydrazine
Purity
95
Packaging
5g
Price
$1417
Updated
2021/12/16
Labseeker
Product number
SC-39255
Product name
1-(1-phenylpropan-2-yl)hydrazine
Purity
95
Packaging
10g
Price
$1767
Updated
2021/12/16
Labseeker
Product number
SC-39255
Product name
1-(1-phenylpropan-2-yl)hydrazine
Purity
95
Packaging
25g
Price
$2567
Updated
2021/12/16
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ALPHA-BROMOISOBUTYRIC ACID Chemical Properties,Usage,Production

Originator

Catron ,Lakeside, US,1959

Definition

ChEBI: Pheniprazine is a member of amphetamines.

Manufacturing Process

A solution containing 741 g (5.0 mols) of 1 -phenyl-2-propylidenylhydrazine, 300 g (5.0 mols) of glacial acetic acid and 900 cc of absolute ethanol was subjected to hydrogenation at 1,875 psi of hydrogen in the presence of 10 g of platinum oxide catalyst and at a temperature of 30°C to 50°C (variation due to exothermic reaction). The catalyst was removed by filtration and the solvent and acetic acid were distilled. The residue was taken up in water and made strongly alkaline by the addition of solid potassium hydroxide. The alkaline mixture was extracted with ether and the ether extracts dried with potassium carbonate. The product was collected by fractional distillation, BP 85°C (0.30 mm); yield 512 g (68%).
The hydrochloride salt was formed in a mixture of 1:10 isopropyl alcohol:diisopropyl ether and recrystallized from acetonitrile, yield 87%, MP 124°C to 125°C.

brand name

Catron Hydrochloride (Marion Merrell Dow).

Therapeutic Function

Antihypertensive

Safety Profile

Poison by ingestion, intraperitoneal, subcutaneous, and intravenous routes. Human systemic effects by an unspecified route: visual field effects. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx.

ALPHA-BROMOISOBUTYRIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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ALPHA-BROMOISOBUTYRIC ACID Suppliers

Shanghai Sunway Pharmaceutical Technology Co.,Ltd.
Tel
021-51816796-820 13611835272
Fax
021-5161 3951
Email
sales2@sunwaypharm.com
Country
China
ProdList
44458
Advantage
58
TargetMol Chemicals Inc.
Tel
15002134094
Email
marketing@targetmol.cn
Country
China
ProdList
19711
Advantage
58
TargetMol Chemicals Inc.
Tel
+8613564774135
Email
zijue.cai@tsbiochem.com
Country
United States
ProdList
19863
Advantage
58