ChemicalBook > CAS DataBase List > 3-chloro-1-(1,1-dimethylethyl)Naphthalene
3-chloro-1-(1,1-dimethylethyl)Naphthalene
- Product Name
- 3-chloro-1-(1,1-dimethylethyl)Naphthalene
- CAS No.
- 2217657-09-3
- Chemical Name
- 3-chloro-1-(1,1-dimethylethyl)Naphthalene
- Synonyms
- 1-(tert-butyl)-3-chloronaphthalene;3-chloro-1-(1,1-dimethylethyl)Naphthalene;Naphthalene, 3-chloro-1-(1,1-dimethylethyl)-
- CBNumber
- CB16199192
- Molecular Formula
- C14H15Cl
- Formula Weight
- 218.72
- MOL File
- 2217657-09-3.mol
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3-chloro-1-(1,1-dimethylethyl)Naphthalene Property
- Boiling point:
- 300.1±11.0 °C(Predicted)
- Density
- 1.081±0.06 g/cm3(Predicted)
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3-chloro-1-(1,1-dimethylethyl)Naphthalene Chemical Properties,Usage,Production
Uses
3-chloro-1-(1,1-dimethylethyl)Naphthalene, also known as 1-(tert-butyl)-3-chloronaphthalene, is a key intermediate in the synthesis process of organic electroluminescent diodes (OLED) molecular materials.
Preparation
In a three-neck flask, the catalyst ligand 1-(2-carboxyethyl)-3-formyltriacyl-1H-imidazol-3-ammonium chloride (1.03 mmol), nickel acetylacetonate (1.01 mmol), and lithium tert-butoxide (31.2 mmol) were added to tetrahydrofuran (100 mL). Isopropyl magnesium chloride (14.6 mL, 1.7 M ether solution, 24.8 mmol) was subsequently added under nitrogen protection and agitation. Add 1-bromo-3-chloronaphthalene after 0.5 h and stir at 0 °C for 2 h. Finally, 3-chloro-1-(1,1-dimethylethyl)Naphthalene was obtained after purification.
3-chloro-1-(1,1-dimethylethyl)Naphthalene Preparation Products And Raw materials
Raw materials
Preparation Products
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