ChemicalBook > CAS DataBase List > 2-(AMINOMETHYL)PHENYL BORONIC ACID

2-(AMINOMETHYL)PHENYL BORONIC ACID

Product Name
2-(AMINOMETHYL)PHENYL BORONIC ACID
CAS No.
248274-03-5
Chemical Name
2-(AMINOMETHYL)PHENYL BORONIC ACID
Synonyms
2-carbomethylphenylboronic acid;2-(AMINOMETHYL)PHENYL BORONIC ACID;2-(Aminomethyl)phenyl boronic acid 95%;Boronic acid, B-[2-(aminomethyl)phenyl]-
CBNumber
CB1722121
Molecular Formula
C7H10BNO2
Formula Weight
150.97
MOL File
248274-03-5.mol
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2-(AMINOMETHYL)PHENYL BORONIC ACID Property

Boiling point:
354.0±44.0 °C(Predicted)
Density 
1.18±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
8.23±0.53(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2931900090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A630763
Product name
2-AminomethylphenylboronicAcid
Packaging
10mg
Price
$120
Updated
2021/12/16
AK Scientific
Product number
Z4493
Product name
(2-(Aminomethyl)phenyl)boronicacid
Packaging
1g
Price
$151
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA140856
Product name
(2-(Aminomethyl)phenyl)boronic acid
Packaging
50mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA140856
Product name
(2-(Aminomethyl)phenyl)boronic acid
Packaging
100mg
Price
$165
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA140856
Product name
(2-(Aminomethyl)phenyl)boronic acid
Packaging
250mg
Price
$300
Updated
2021/12/16
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2-(AMINOMETHYL)PHENYL BORONIC ACID Chemical Properties,Usage,Production

Synthesis

138642-62-3

248274-03-5

The general procedure for the synthesis of (2-(aminomethyl)phenyl)boronic acid from 2-cyanophenylboronic acid was as follows: to a methanol solution (20 mL) containing 2-cyanophenylboronic acid (300 mg, 2.0 mmol) was added nickel ryenne (100 mg, 10% w/w). The reaction mixture was stirred for 4 h at room temperature under hydrogen pressure of 50 psi. Upon completion of the reaction, the reaction mixture was filtered through a diatomaceous earth pad and the filtrate was concentrated under vacuum to afford (2-(aminomethyl)phenyl)boronic acid 150 mg (48.7% yield) as a white solid. Mass spectrum (electrospray positive ion mode): m/z = 152.20, 153.40, 154.35, 155.65 [M + H]+. Analyzed by liquid chromatography-mass spectrometry: retention time tR = 0.76 min.

References

[1] Patent: WO2015/81280, 2015, A1. Location in patent: Paragraph 00497; 00498

2-(AMINOMETHYL)PHENYL BORONIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-(AMINOMETHYL)PHENYL BORONIC ACID manufacturers

Career Henan Chemical Co
Product
2-(AMINOMETHYL)PHENYL BORONIC ACID 248274-03-5
Price
US $1.00/KG
Min. Order
1KG
Purity
98%-100%
Supply Ability
1
Release date
2018-08-12