ChemicalBook > CAS DataBase List > 3-CHLORO-4-METHOXYBENZALDEHYDE

3-CHLORO-4-METHOXYBENZALDEHYDE

Product Name
3-CHLORO-4-METHOXYBENZALDEHYDE
CAS No.
13726-16-4
Chemical Name
3-CHLORO-4-METHOXYBENZALDEHYDE
Synonyms
AKOS B029259;CHEMBRDG-BB 6945816;TIMTEC-BB SBB003854;3-CHLORO-P-ANISALDEHYDE;3-CHLORO-4-METHOXYBENZALDEHYDE;3-Methoxy-4-chlorobenzaldehyde;Benzaldehyde, 4-chloro-3-methoxy-;3-CHLORO-4-METHOXYBENZENECARBALDEHYDE
CBNumber
CB1727999
Molecular Formula
C8H7ClO2
Formula Weight
170.59
MOL File
13726-16-4.mol
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3-CHLORO-4-METHOXYBENZALDEHYDE Property

Melting point:
56-60 °C(lit.)
Boiling point:
265℃
Density 
1.244
Flash point:
118℃
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
Powder
color 
White to pale brown
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Safety

Hazard Codes 
Xi
Safety Statements 
22-24/25
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
2912490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
C596648
Product name
4-Chloro-3-methoxybenzaldehyde
Packaging
50mg
Price
$60
Updated
2021/12/16
TRC
Product number
C596648
Product name
4-Chloro-3-methoxybenzaldehyde
Packaging
100mg
Price
$75
Updated
2021/12/16
Rieke Metals
Product number
AL0086
Product name
4-Chloro-3-methoxybenzaldehyde
Packaging
5g
Price
$87
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC55641
Product name
4-Chloro-3-methoxybenzaldehyde
Packaging
250mg
Price
$70
Updated
2021/12/16
Matrix Scientific
Product number
054394
Product name
4-Chloro-3-methoxybenzaldehyde
Purity
97%
Packaging
5g
Price
$35
Updated
2021/12/16
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3-CHLORO-4-METHOXYBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

13726-17-5

13726-16-4

D. General procedure for synthesizing 4-chloro-3-methoxybenzaldehyde: Manganese dioxide (5.65 g, 65 mmol) was added to a solution of (4-chloro-3-methoxyphenyl)methanol (5.08 g, 29.4 mmol) in benzene (120 mL). The reaction mixture was refluxed for 17 h. After cooling, the reaction mixture was filtered through diatomaceous earth and the filter cake was washed with dichloromethane (300 mL). The filtrate was concentrated under reduced pressure to give 4-chloro-3-methoxybenzaldehyde (4.5 g, 89% yield).

References

[1] Journal of Medicinal Chemistry, 1992, vol. 35, # 23, p. 4408 - 4414
[2] Patent: US2002/77486, 2002, A1
[3] Patent: US6906063, 2005, B2
[4] Patent: EP2314593, 2016, B1. Location in patent: Paragraph 0202
[5] Tetrahedron Letters, 2005, vol. 46, # 32, p. 5417 - 5419

3-CHLORO-4-METHOXYBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-CHLORO-4-METHOXYBENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
3-CHLORO-4-METHOXYBENZALDEHYDE 13726-16-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98% HPLC
Supply Ability
10 tons
Release date
2020-02-01