ChemicalBook > CAS DataBase List > 8-Methylene-1,4-dioxa-spiro[4.5]decane

8-Methylene-1,4-dioxa-spiro[4.5]decane

Product Name
8-Methylene-1,4-dioxa-spiro[4.5]decane
CAS No.
51656-90-7
Chemical Name
8-Methylene-1,4-dioxa-spiro[4.5]decane
Synonyms
8-METHYLENE-1,4-DIOXA-SPIRO[4.5]DECANE;8-METHYLENE-l, 4-DI0XASPIR0[4. 5]DECANE;1,4-Dioxaspiro[4.5]decane, 8-methylene-
CBNumber
CB1767597
Molecular Formula
C9H14O2
Formula Weight
154.21
MOL File
Mol file
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8-Methylene-1,4-dioxa-spiro[4.5]decane Property

Boiling point:
221.4±40.0 °C(Predicted)
Density 
1.04±0.1 g/cm3(Predicted)
InChI
InChI=1S/C9H14O2/c1-8-2-4-9(5-3-8)10-6-7-11-9/h1-7H2
InChIKey
BCWKBPCNPHCCQS-UHFFFAOYSA-N
SMILES
O1C2(CCC(=C)CC2)OCC1
CAS DataBase Reference
51656-90-7
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Safety

HS Code 
2932990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M223065
Product name
8-Methylene-1,4-dioxaspiro[4.5]decane
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
M223065
Product name
8-Methylene-1,4-dioxaspiro[4.5]decane
Packaging
50mg
Price
$175
Updated
2021/12/16
AK Scientific
Product number
3099AL
Product name
8-Methylene-1,4-dioxaspiro[4.5]decane
Packaging
1g
Price
$424
Updated
2021/12/16
Apolloscientific
Product number
OR451154
Product name
8-Methylene-1,4-dioxa-spiro[4.5]decane
Packaging
1g
Price
$501
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0361777
Product name
8-METHYLENE-1,4-DIOXASPIRO[4.5]DECANE
Purity
95.00%
Packaging
5MG
Price
$504.16
Updated
2021/12/16
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8-Methylene-1,4-dioxa-spiro[4.5]decane Chemical Properties,Usage,Production

Synthesis

Add BuLi to a solution of methyl triphenylphosphonium bromide in THF at -78° C. Stir this suspension for 10 min at -78° C, then 30 min at 0° C. Cool the orange solution obtained to -78° C, and add a solution of the monoethylene ketal of 1,4-cyclohexanedione in THF. Stir the reaction mixture overnight at room temperature (RT), then filter on Celite. Rinse the solid with pentane. After evaporating the solvents, the residue on the silica gel was chromatographed. 8-Methylene-1,4-dioxa-spiro[4.5]decane is thus obtained (colorless oil).

8-Methylene-1,4-dioxa-spiro[4.5]decane Preparation Products And Raw materials

Raw materials

Preparation Products

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51656-90-7, 8-Methylene-1,4-dioxa-spiro[4.5]decaneRelated Search:


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