ChemicalBook > CAS DataBase List > ETHYL 2-AMINO-4-FLUOROBENZOATE
ETHYL 2-AMINO-4-FLUOROBENZOATE
- Product Name
- ETHYL 2-AMINO-4-FLUOROBENZOATE
- CAS No.
- 117324-05-7
- Chemical Name
- ETHYL 2-AMINO-4-FLUOROBENZOATE
- Synonyms
- amino-Ethyl 2-Ethyl 2-ami-4-fluorobenzoate;ETHYL 2-AMINO-4-FLUOROBENZOATE;-amino-4-fluoro-benzoic acid ethyl ester;Benzoic acid, 2-amino-4-fluoro-, ethyl ester
- CBNumber
- CB1769571
- Molecular Formula
- C9H10FNO2
- Formula Weight
- 183.18
- MOL File
- 117324-05-7.mol
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ETHYL 2-AMINO-4-FLUOROBENZOATE Property
- Boiling point:
- 271.2±20.0 °C(Predicted)
- Density
- 1.218±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 1.46±0.10(Predicted)
- Appearance
- Light yellow to brown Solid
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Safety
- HS Code
- 2916399090
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N-Bromosuccinimide Price
TRC
- Product number
- E899895
- Product name
- Ethyl2-Amino-4-fluorobenzoate
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
Apolloscientific
- Product number
- PC201039
- Product name
- Ethyl2-amino-4-fluorobenzoate
- Purity
- 98%
- Packaging
- 1g
- Price
- $106
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 083311
- Product name
- Ethyl 2-amino-4-fluorobenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $168
- Updated
- 2021/12/16
Apolloscientific
- Product number
- PC201039
- Product name
- Ethyl2-amino-4-fluorobenzoate
- Purity
- 98%
- Packaging
- 5g
- Price
- $315
- Updated
- 2021/12/16
AK Scientific
- Product number
- Z3932
- Product name
- Ethyl2-amino-4-fluorobenzoate
- Packaging
- 5g
- Price
- $325
- Updated
- 2021/12/16
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ETHYL 2-AMINO-4-FLUOROBENZOATE Chemical Properties,Usage,Production
Synthesis
446-32-2
117324-05-7
A. Synthesis of ethyl 2-amino-4-fluorobenzoate 2-Amino-4-fluorobenzoic acid (1.57 g, 10.1 mmol) was dissolved in anhydrous ethanol (20 mL) and cooled to low temperature. Pure thionyl chloride (4.4 mL, 60 mmol) was added slowly and the reaction mixture was refluxed for 4 days. Subsequently, thionyl chloride (8 mL, 110 mmol) was added supplementally and the mixture was concentrated after the reaction was completed. It was diluted with ethyl acetate (EtOAc), washed with 2N sodium hydroxide (NaOH) solution, dried and concentrated in vacuum to give ethyl 2-amino-4-fluorobenzoate (1.73 g, 94% yield).
References
[1] Patent: US2002/77486, 2002, A1
[2] Patent: US6906063, 2005, B2
[3] Patent: EP1380576, 2004, A1. Location in patent: Page 97
ETHYL 2-AMINO-4-FLUOROBENZOATE Preparation Products And Raw materials
Raw materials
Preparation Products
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117324-05-7, ETHYL 2-AMINO-4-FLUOROBENZOATERelated Search:
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