4,4'-oxybisbutan-2-ol
- Product Name
- 4,4'-oxybisbutan-2-ol
- CAS No.
- 821-33-0
- Chemical Name
- 4,4'-oxybisbutan-2-ol
- Synonyms
- Diskin;Boutybil;Dis-Cinil;Diskinebyl;Colenormol;Dyskinebyl;Einecs 212-475-3;5-Oxa-2,8-nonandiol;4,4'-oxydi-2-butanol;4,4'-oxybisbutan-2-ol
- CBNumber
- CB1903135
- Molecular Formula
- C8H18O3
- Formula Weight
- 162.23
- MOL File
- 821-33-0.mol
4,4'-oxybisbutan-2-ol Property
- Melting point:
- <25 °C
- Boiling point:
- 278.4±15.0 °C(Predicted)
- Density
- 0.997±0.06 g/cm3(Predicted)
- pka
- 14.65±0.20(Predicted)
- EPA Substance Registry System
- 2-Butanol, 4,4'-oxybis- (821-33-0)
4,4'-oxybisbutan-2-ol Chemical Properties,Usage,Production
Originator
Dyskineacutebyl,Saunier
Definition
ChEBI: Oxydibutanol is a secondary alcohol.
Manufacturing Process
To a solution of 3 mols butylmagnesiumbromide in ether was added dropwise an one mol of β-cyanoethyloxide. The mixture was refluxed for 1 hour. Then after cooling to the mixture was added hydrochloric acid. An organic layer was dried under sodium sulfate and evaporated. An oil layer was distilled in vacuum. The oxo-3-butane oxide has a boiling point 123-125°C at 15 mm. A mixture of 100 g of oxo-3-butane oxide, 500 ml ethanol and 15 g Nickel Reney was loaded in autoclave and heated at 45-50°C. In autoclave was introduced a hydrogene. After cooling the mixture was filtered and ethanol was distilled off. 1,1'-Dimethyl-3,3'-oxydipropanol was distilled at 160161°C/18 mm.
Therapeutic Function
Choleretic, Spasmolytic
4,4'-oxybisbutan-2-ol Preparation Products And Raw materials
Raw materials
Preparation Products
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