perhydroacenaphthene
- Product Name
- perhydroacenaphthene
- CAS No.
- 2146-36-3
- Chemical Name
- perhydroacenaphthene
- Synonyms
- Decahydroacenaphthene;Dodecahydroacenaphthylene;Einecs 218-412-6;perhydroacephthene;Perhydroacenaphthyle;perhydroacenaphthene;Acenaphthylene, dodecahydro-;Tricyclo[7.2.1.05,12]dodecane;Tricyclo(6,3,1,04,12)dodecane;Perhydroacenaphthene 2146-36-3 Decahydroacenaphthene
- CBNumber
- CB1933376
- Molecular Formula
- C12H20
- Formula Weight
- 164.29
- MOL File
- 2146-36-3.mol
perhydroacenaphthene Property
- Melting point:
- 36℃
- Boiling point:
- 235℃
- Density
- 1.029 g/cm3
- refractive index
- 1.577 (589.3 nm 20℃)
- storage temp.
- 2-8°C
- form
- Liquid
- color
- Yellowish brown
- EPA Substance Registry System
- Acenaphthylene, dodecahydro- (2146-36-3)
N-Bromosuccinimide Price
- Product number
- CD41001589
- Product name
- Dodecahydroacenaphthylene
- Purity
- 90%
- Packaging
- 25g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CD41001589
- Product name
- Dodecahydroacenaphthylene
- Purity
- 90%
- Packaging
- 100g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- 2146363
- Product name
- Dodecahydroacenaphthylene
- Packaging
- 100g
- Price
- $400
- Updated
- 2021/12/16
perhydroacenaphthene Chemical Properties,Usage,Production
Uses
Perhydroacenaphthene or dodecahydroacenaphthylene is used in the synthesis of Alkyladamantanes by the passage of the latter over the alumina catalyst in a flow-type plant with a metal reactor that has application in the field of nanotechnology.
Preparation
Perhydro acenaphthene is the main raw material of preparation 1,3-dimethyladamantane, is the important intermediate of preparation Derivatives of Adamantane.Derivatives of Adamantane is a kind of excellent antidementia agent, clinical research confirmation its have good efficacy to vascular dementia.
The synthesis of Perhydroacenaphthene:
1) adding industrial acenaphthylene to 95% ethanol, heating, refluxing and dissolving, then cooling, crystallizing, centrifuging to obtain refined acenaphthene, and carrying out distillation recycling of the filtrate;
2) adding the refined acenaphthene and a catalyst Raney Ni into a high-pressure kettle, replacing gas in the kettle with hydrogen, filling hydrogen to make the pressure in the kettle rise to 0.8 MPa, heating up to about 180 DEG C, starting a reaction for 5 h, continuously supplementing hydrogen during the reaction, making the pressure in the kettle rise slowly, and allowing the pressure after the reaction to be 4.0 MPa;
3) cooling after the reaction is finished, filtering the catalyst, and thus obtaining the perhydroacenaphthene.
https://patents.google.com/patent/CN105461499A/en
perhydroacenaphthene Preparation Products And Raw materials
Raw materials
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View Lastest Price from perhydroacenaphthene manufacturers
- Product
- Perhydroacenaphthene 2146-36-3 Decahydroacenaphthene 2146-36-3
- Price
- US $9.55/KG
- Min. Order
- 1KG
- Purity
- 99.50% IN STOCK
- Supply Ability
- 350 MT per month
- Release date
- 2019-09-05