ChemicalBook > CAS DataBase List > 2-Amino-4-chloro-6-picoline

2-Amino-4-chloro-6-picoline

Product Name: 2-Amino-4-chloro-6-picoline
CAS No.: 36340-61-1
Chemical Name: 2-Amino-4-chloro-6-picoline
Synonyms: oro-6-picoL;6-AMINO-4-CHLORO-2-PICOLINE;2-Amino-4-chloro-6-picoline;4-chloro-6-Methyl-2-PyridinaMine;2-AMino-4-chloro-6-Methylpyridine;4-Chloro-6-methylpyridin-2-ylamine;2-Pyridinamine, 4-chloro-6-methyl-;2-Amino-4-chloro-6-picoline ISO 9001：2015 REACH
CBNumber: CB1947100
Molecular Formula: C6H7ClN2
Formula Weight: 142.59
MOL File: 36340-61-1.mol

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2-Amino-4-chloro-6-picoline Property

Melting point:: 108-109 °C
Boiling point:: 245.1±35.0 °C(Predicted)
Density: 1.260±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 5.96±0.35(Predicted)
color: Grey
InChI: InChI=1S/C6H7ClN2/c1-4-2-5(7)3-6(8)9-4/h2-3H,1H3,(H2,8,9)
InChIKey: IKKMKJOVXQEEHS-UHFFFAOYSA-N
SMILES: C1(N)=NC(C)=CC(Cl)=C1
CAS DataBase Reference: 36340-61-1

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A595890
Product name: 2-Amino-4-chloro-6-picoline
Packaging: 50mg
Price: $90
Updated: 2021/12/16

Biosynth Carbosynth

Product number: NA66773
Product name: 2-Amino-4-chloro-6-methylpyridine
Packaging: 500g
Price: $100
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-5-8G
Product name: 4-Chloro-6-methylpyridin-2-amine
Purity: 97%
Packaging: 250mg
Price: $119
Updated: 2021/12/16

Biosynth Carbosynth

Product number: NA66773
Product name: 2-Amino-4-chloro-6-methylpyridine
Packaging: 1g
Price: $150
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-5-8G
Product name: 4-Chloro-6-methylpyridin-2-amine
Purity: 97%
Packaging: 5G
Price: $791
Updated: 2021/12/16

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2-Amino-4-chloro-6-picoline Chemical Properties,Usage,Production

Synthesis

823-96-1

116632-24-7

36340-61-1

The general procedure for the synthesis of 2-amino-4-chloro-6-methylpyridine from 2-amino-4,6-dichloropyridine and trimethylcyclotriboroxane is as follows: to a 10% aqueous solution of dioxane (0.1 M) were added sequentially 2-amino-4,6-dichloropyridine (1.0 eq.), trimethylcyclotriboroxane (1.5 eq.), tetrakis(triphenylphosphine)palladium (0.10 eq.) and potassium carbonate (3.0 eq.). The reaction mixture was heated to 120 °C in an oil bath with continuous stirring for 18 hours. Upon completion of the reaction, it was cooled to room temperature (note: not all ingredients were completely consumed). The reaction mixture was extracted with ethyl acetate and the organic phase was dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using 5% methanol/dichloromethane as eluent, resulting in an off-white 2-amino-4-chloro-6-methylpyridine solid in 23% yield.LCMS analysis showed a molecular ion peak (m/z) of 143 (MH+) for the target compound with a retention time (Rt) of 1.11 min on the liquid chromatogram.

References

[1] Patent: US2011/195980, 2011, A1. Location in patent: Page/Page column 15

2-Amino-4-chloro-6-picoline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Amino-4-chloro-6-picoline manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2-Amino-4-chloro-6-picoline 36340-61-1
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-18

Dideu Industries Group Limited

Product: 2-Amino-4-chloro-6-picoline 36340-61-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-30

Career Henan Chemical Co

Product: 2-Amino-4-chloro-6-picoline 36340-61-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-24

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2-Amino-4-chloro-6-picoline ISO 9001：2015 REACH

36340-61-1