2-amino-4-chlorobenzamide
Uses- Product Name
- 2-amino-4-chlorobenzamide
- CAS No.
- 5900-59-4
- Chemical Name
- 2-amino-4-chlorobenzamide
- Synonyms
- 4-Chloroanthranilamide;2-aMino-4-chlrobenzaMide;2-amino-4-chlorobenzamide;Benzamide, 2-amino-4-chloro-;2-amino-4-chlorophenylformamide;2-amino-4-chlorobenzamide(SALTDATA: FREE)
- CBNumber
- CB21016392
- Molecular Formula
- C7H7ClN2O
- Formula Weight
- 170.6
- MOL File
- 5900-59-4.mol
2-amino-4-chlorobenzamide Property
- Melting point:
- 181.5 °C
- Boiling point:
- 308.8±27.0 °C(Predicted)
- Density
- 1.394±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- solid
- pka
- 15.48±0.50(Predicted)
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H317May cause an allergic skin reaction
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P272Contaminated work clothing should not be allowed out of the workplace.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- BBO000415
- Product name
- 2-Amino-4-chlorobenzamide
- Packaging
- 1 g
- Price
- $259
- Updated
- 2025/07/31
- Product number
- A620193
- Product name
- 2-Amino-4-chlorobenzamide
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- A620193
- Product name
- 2-Amino-4-chlorobenzamide
- Packaging
- 5g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- FA140221
- Product name
- 2-Amino-4-chlorobenzamide
- Packaging
- 2g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- J55327
- Product name
- 2-Amino-4-chlorobenzamide
- Packaging
- 10g
- Price
- $100
- Updated
- 2021/12/16
2-amino-4-chlorobenzamide Chemical Properties,Usage,Production
Uses
2-Amino-4-chlorobenzamide is a useful research chemical.
Synthesis
89-77-0
5900-59-4
Method I: Synthesis of 2-amino-4-chlorobenzamide (ii-b) 1. 2-Amino-4-chlorobenzoic acid (3.42 g, 20 mmol) was dissolved in DMF (45 mL) and HOBt (2.70 g, 20 mmol) was added. 2. After stirring for 10 min, EDC-HCl (3.82 g, 20 mmol) was added to the mixture. 3. the reaction mixture was stirred at room temperature for 2 hr. 4. NH4OH (28%, 5 mL) was slowly added at 0 °C with vigorous stirring. 5. After addition, continue stirring at room temperature for 2 hours. 6. The reaction mixture was added slowly dropwise to water (200 mL) and a precipitate was precipitated. 7. The precipitate was collected by filtration and dried under vacuum to give 2.98 g of the target product ii-b as a gray solid in 87.6% yield. 8. 8. The product was characterized by LCMS m/z = 171.0 (M + 1), 173.0 (M + 3) (Method B) (retention time = 1.39 min). 1H NMR (400 MHz, DMSO-d6): δ 7.27 (d, J = 9.6 Hz, 1H), 6.68 (d, J = 2.4 Hz, 1H), 6.60 (dd, J = 8.4, 2.0 Hz, 1H), 5.50-5.82 (m, 4H).
References
[1] European Journal of Medicinal Chemistry, 2018, vol. 157, p. 1361 - 1375
[2] Patent: US2015/307477, 2015, A1. Location in patent: Paragraph 1473
[3] Patent: JP6121658, 2017, B2. Location in patent: Paragraph 1063; 1064; 1065
[4] Patent: WO2010/99379, 2010, A1. Location in patent: Page/Page column 142
[5] Arkivoc, 2012, vol. 2012, # 8, p. 198 - 213
2-amino-4-chlorobenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-amino-4-chlorobenzamide manufacturers
- Product
- 2-amino-4-chlorobenzamide 5900-59-4
- Price
- US $5.00/ASSAYS
- Min. Order
- 1ASSAYS
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2019-08-05