ChemicalBook > CAS DataBase List > Benzenemethanol, 2-amino-3-methoxy- (9CI)

Benzenemethanol, 2-amino-3-methoxy- (9CI)

Product Name: Benzenemethanol, 2-amino-3-methoxy- (9CI)
CAS No.: 205877-13-0
Chemical Name: Benzenemethanol, 2-amino-3-methoxy- (9CI)
Synonyms: 2-Amino-3-methoxybenzyl Alcohol;2-Amino-3-methoxybenzenemethanol;Benzenemethanol, 2-amino-3-methoxy-;Benzenemethanol, 2-amino-3-methoxy- (9CI)
CBNumber: CB21041891
Molecular Formula: C8H11NO2
Formula Weight: 153.18
MOL File: 205877-13-0.mol

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Benzenemethanol, 2-amino-3-methoxy- (9CI) Property

Melting point:: 38 °C
Boiling point:: 312.6±27.0 °C(Predicted)
Density: 1.182±0.06 g/cm3(Predicted)
storage temp.: 2-8°C, protect from light
pka: 14.28±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0371219
Product name: (2-AMINO-3-METHOXY-PHENYL)-METHANOL
Purity: 95.00%
Packaging: 5MG
Price: $495.9
Updated: 2021/12/16

AK Scientific

Product number: 6961CC
Product name: (2-Amino-3-methoxyphenyl)methanol
Packaging: 1g
Price: $802
Updated: 2021/12/16

Chemenu

Product number: CM116437
Product name: 2-Amino-3-methoxybenzylAlcohol
Purity: 95%
Packaging: 1g
Price: $307
Updated: 2021/12/16

Acrotein

Product number: AC-6784
Product name: 2-Amino-3-methoxybenzenemethanol
Purity: 97%
Packaging: 1g
Price: $366.67
Updated: 2021/12/16

Abosyn

Product number: 61-10217
Product name: (2-Amino-3-methoxyphenyl)methanol
Purity: 95-98%
Packaging: 1g
Price: $405
Updated: 2021/12/16

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Benzenemethanol, 2-amino-3-methoxy- (9CI) Chemical Properties,Usage,Production

Synthesis

3177-80-8

205877-13-0

General method: 1.08 M THF solution of borane-tetrahydrofuran complex (24.3 mL, 26.2 mmol) of 2-amino-3-methoxybenzoic acid (1.5 g, 8.74 mmol) was slowly added dropwise to a solution of tetrahydrofuran (THF, 5 mL) at 0 °C under argon protection for a controlled time of 10 min. After the dropwise addition was completed, the reaction mixture was warmed up to 30 °C and stirred continuously for 1.5 hours. After completion of the reaction, the solution was cooled to 0 °C, a mixed solution of tetrahydrofuran and water (THF/H2O = 1:1, 60 mL) and potassium carbonate was added, followed by extraction with ether three times. The organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was recrystallized by ethyl acetate to give (2-amino-3-methoxy-phenyl)-methanol (1a, 1.2 g, 88% yield) as white needle-like crystals.

References

[1] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 19, p. 5810 - 5831
[2] Journal of the Chemical Society - Perkin Transactions 1, 1998, # 7, p. 1193 - 1202
[3] Journal of Medicinal Chemistry, 2005, vol. 48, # 6, p. 2080 - 2092
[4] Journal of Medicinal Chemistry, 2002, vol. 45, # 15, p. 3280 - 3285
[5] Angewandte Chemie - International Edition, 2016, vol. 55, # 49, p. 15272 - 15276

Benzenemethanol, 2-amino-3-methoxy- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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205877-13-0, Benzenemethanol, 2-amino-3-methoxy- (9CI)Related Search:

Benzenemethanol, 2-amino-3-methoxy- (9CI)

2-Amino-3-methoxybenzenemethanol

2-Amino-3-methoxybenzyl Alcohol

Benzenemethanol, 2-amino-3-methoxy-

205877-13-0

METHOXY