4-Bromo-3,5-dimethylaniline

Uses

Product Name: 4-Bromo-3,5-dimethylaniline
CAS No.: 59557-90-3
Chemical Name: 4-Bromo-3,5-dimethylaniline
Synonyms: 4-Bromo-3,5-xylidine;5-Amino-2-bromo-m-xylene;4-BROMO-3,5-DIMETHYLANILINE;4-Bromo-3,5-dimethylbenzenamine;4-Bromo-3,5-dimethylaniline, 97%;BenzenaMine, 4-broMo-3,5-diMethyl-
CBNumber: CB21091306
Molecular Formula: C8H10BrN
Formula Weight: 200.08
MOL File: 59557-90-3.mol

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4-Bromo-3,5-dimethylaniline Property

Melting point:: 73-74°C
Boiling point:: 261.0±35.0 °C(Predicted)
Density: 1.424±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 4.14±0.10(Predicted)
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C8H10BrN/c1-5-3-7(10)4-6(2)8(5)9/h3-4H,10H2,1-2H3
InChIKey: OGBPXDJLNYCSJH-UHFFFAOYSA-N
SMILES: C1(N)=CC(C)=C(Br)C(C)=C1

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B699715
Product name: 4-Bromo-3,5-dimethylaniline
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B699715
Product name: 4-Bromo-3,5-dimethylaniline
Packaging: 50mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 061258
Product name: (4-Bromo-3,5-dimethylphenyl)amine
Packaging: 5g
Price: $61
Updated: 2021/12/16

AK Scientific

Product number: W7239
Product name: 4-Bromo-3,5-dimethylaniline
Packaging: 5g
Price: $80
Updated: 2021/12/16

Oakwood

Product number: 091982
Product name: 4-Bromo-3,5-dimethylaniline
Purity: 99%
Packaging: 1g
Price: $20
Updated: 2021/12/16

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4-Bromo-3,5-dimethylaniline Chemical Properties,Usage,Production

Uses

4-Bromo-3,5-dimethylaniline is used in organic synthesis and can be used in laboratory research and development processes as well as in chemical and pharmaceutical synthesis.

Synthesis

To a solution of 3,5-dimethylaniline (80 g, 660 mmol) in 800 mL MeCN was added a solution of NBS (117g, 660mmol) in 400 ml MeCN at an ice bath, stirred at room temperature for 16h. The reaction mixture was concentrated under reduced pressure. The residue was purified by silica column chromatography (Eluent C) to give title product 4-bromo-3,5-dimethylaniline 1b (90 g, yellow solid), yield 68.2 %.

References

[1] Journal of Organic Chemistry, 2004, vol. 69, # 15, p. 5065 - 5070
[2] Patent: WO2006/138350, 2006, A2. Location in patent: Page/Page column 196
[3] Canadian Journal of Chemistry, 2009, vol. 87, # 2, p. 440 - 447
[4] Patent: EP3042907, 2016, A1. Location in patent: Paragraph 0257; 0258
[5] Patent: US2012/28923, 2012, A1. Location in patent: Page/Page column 47

4-Bromo-3,5-dimethylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Bromo-3,5-dimethylaniline Suppliers

China 153 France 1 India 4 Ukraine 1 United Kingdom 1 United States 9 Global 169

Hangzhou Dongyan Chemical Co., Ltd.

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Shanghai Harvest Chemical Industrial Co., Ltd.

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ZEROSCHEM.CO.,LTD.

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View Lastest Price from 4-Bromo-3,5-dimethylaniline manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-BROMO-3,5-DIMETHYLANILINE 59557-90-3
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-11

Career Henan Chemical Co

Product: 4-BROMO-3,5-DIMETHYLANILINE 59557-90-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500kg
Release date: 2018-08-19

59557-90-3, 4-Bromo-3,5-dimethylanilineRelated Search:

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4-Bromo-3,5-dimethylbenzenamine

4-Bromo-3,5-xylidine

5-Amino-2-bromo-m-xylene

BenzenaMine, 4-broMo-3,5-diMethyl-

4-BROMO-3,5-DIMETHYLANILINE

4-Bromo-3,5-dimethylaniline, 97%

59557-90-3