ChemicalBook > CAS DataBase List > 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID

2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID

Product Name: 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID
CAS No.: 1003709-47-4
Chemical Name: 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID
Synonyms: 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID;Benzoic acid, 2-bromo-4-fluoro-6-methyl-
CBNumber: CB21091715
Molecular Formula: C8H6BrFO2
Formula Weight: 233.03
MOL File: Mol file

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2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID Property

Boiling point:: 306.6±42.0 °C(Predicted)
Density: 1.680±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 2.53±0.37(Predicted)
Appearance: Light brown to off-white Solid
InChI: InChI=1S/C8H6BrFO2/c1-4-2-5(10)3-6(9)7(4)8(11)12/h2-3H,1H3,(H,11,12)
InChIKey: VOFBSAUUUDKWGR-UHFFFAOYSA-N
SMILES: C(O)(=O)C1=C(C)C=C(F)C=C1Br

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: X4312
Product name: 2-Bromo-4-fluoro-6-methylbenzoicacid
Packaging: 250mg
Price: $136
Updated: 2021/12/16

AK Scientific

Product number: X4312
Product name: 2-Bromo-4-fluoro-6-methylbenzoicacid
Packaging: 1g
Price: $246
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0065957
Product name: 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $504.06
Updated: 2021/12/16

Ambeed

Product number: A134853
Product name: 2-Bromo-4-fluoro-6-methylbenzoicacid
Purity: 97%
Packaging: 100mg
Price: $30
Updated: 2021/12/16

Ambeed

Product number: A134853
Product name: 2-Bromo-4-fluoro-6-methylbenzoicacid
Purity: 97%
Packaging: 250mg
Price: $40
Updated: 2021/12/16

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2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

1262396-02-0

1003709-47-4

The general procedure for the synthesis of 2-bromo-4-fluoro-6-methylbenzoic acid from the compound (CAS: 1262396-02-0) was as follows: 2-bromo-4-fluoro-6-methylbenzamide (0.9 g, 3.9 mmol) was dissolved in 75% aqueous sulfuric acid (4 mL) and heated to 80 °C. Sodium nitrite (0.5 g, 7.2 mmol) was added slowly over a period of 1 h. Continuous generation of nitrogen dioxide gas was observed during the reaction. Upon completion of the reaction, the mixture was cooled to 20 °C and diluted by adding cold water (15 mL). The product was extracted several times with ethyl acetate (6 x 2 mL). The organic phases were combined, washed sequentially with water (4 × 2 mL) and brine (2 × 2 mL), dried over anhydrous sodium sulfate, filtered and concentrated to give 0.879 g of pure 2-bromo-4-fluoro-6-methylbenzoic acid in 97% yield. The product was characterized by 1H NMR (400 MHz, DMSO-d6) and 13C NMR (300 MHz, DMSO-d6 + CCl4), and the data were consistent with the expected structure.

References

[1] Patent: WO2011/6803, 2011, A1. Location in patent: Page/Page column 35
[2] Patent: WO2014/64149, 2014, A1. Location in patent: Page/Page column 27; 28

2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID manufacturers

Career Henan Chemical Co

Product: 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACID 1003709-47-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-20

1003709-47-4, 2-BROMO-4-FLUORO-6-METHYLBENZOIC ACIDRelated Search:

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