4-(2-Bromo-acetyl)-benzoic acid

Product Name: 4-(2-Bromo-acetyl)-benzoic acid
CAS No.: 20099-90-5
Chemical Name: 4-(2-Bromo-acetyl)-benzoic acid
Synonyms: Benzoic acid,4-(2-bromoacetyl)-;2-BroMo-4'-(hydroxycarbonyl)acetophenone
CBNumber: CB21113244
Molecular Formula: C9H7BrO3
Formula Weight: 243.05
MOL File: 20099-90-5.mol

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4-(2-Bromo-acetyl)-benzoic acid Property

Melting point:: 224-225℃ (methanol )
Boiling point:: 386.2±22.0 °C(Predicted)
Density: 1.657±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: 3.68±0.10(Predicted)
color: Off-white

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Safety

RIDADR: 1759
HazardClass: 8
PackingGroup: Ⅲ
HS Code: 2918290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B679250
Product name: 4-(2-Bromoacetyl)benzoicAcid
Packaging: 100mg
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19186
Product name: 4-(2-Bromoacetyl)benzoic acid
Packaging: 500mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19186
Product name: 4-(2-Bromoacetyl)benzoic acid
Packaging: 1g
Price: $85
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19186
Product name: 4-(2-Bromoacetyl)benzoic acid
Packaging: 2g
Price: $136
Updated: 2021/12/16

AK Scientific

Product number: J55496
Product name: 4-(2-Bromoacetyl)benzoicacid
Packaging: 10g
Price: $150
Updated: 2021/12/16

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4-(2-Bromo-acetyl)-benzoic acid Chemical Properties,Usage,Production

Uses

A phenacyl bromide

Synthesis

586-89-0

20099-90-5

General procedure for the synthesis of 4-(2-bromoacetyl)benzoic acid from 4-acetylbenzoic acid: 1 mmol of 4-acetylbenzoic acid was dissolved in 10 mL of acetic acid (AcOH). Subsequently, 1 equivalent of bromine was dissolved in 10 mL of acetic acid (AcOH) and added dropwise to the reaction mixture. The reaction mixture was stirred at room temperature for 4 hours. After completion of the reaction, the solvent was evaporated to dryness. The product was purified by normal phase column chromatography using a gradient increasing dichloromethane solution of methanol as eluent.

References

[1] Journal of the American Chemical Society, 2000, vol. 122, # 39, p. 9361 - 9366
[2] European Journal of Medicinal Chemistry, 2014, vol. 77, p. 361 - 377
[3] Russian Journal of Applied Chemistry, 2007, vol. 80, # 4, p. 571 - 575
[4] Bioorganic and Medicinal Chemistry, 1997, vol. 5, # 3, p. 601 - 621
[5] Journal of Medicinal Chemistry, 2005, vol. 48, # 24, p. 7520 - 7534

4-(2-Bromo-acetyl)-benzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(2-Bromo-acetyl)-benzoic acid Suppliers

Canada 1 China 86 India 4 Russia 1 United Kingdom 2 United States 8 Global 102

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View Lastest Price from 4-(2-Bromo-acetyl)-benzoic acid manufacturers

Career Henan Chemical Co

Product: 4-(2-Bromo-acetyl)-benzoic acid 20099-90-5
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 100KG
Release date: 2018-12-22

20099-90-5, 4-(2-Bromo-acetyl)-benzoic acidRelated Search:

4-(2-BROMO-PENTANOYL)-BENZOIC ACIDMETHYL ESTER 4-(2-BROMOETHYL)BENZOIC ACID 4-Acetylbenzoic acid 4-(2-Bromo-acetyl)-benzoic acid 2-Bromo-4'-methylacetophenone 4-(2-BROMO-ACETYL)-BENZOIC ACID METHYL ESTER

2-BroMo-4'-(hydroxycarbonyl)acetophenone

Benzoic acid,4-(2-bromoacetyl)-

20099-90-5

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