3,5-Dichlorobenzyl bromide
- Product Name
- 3,5-Dichlorobenzyl bromide
- CAS No.
- 7778-01-0
- Chemical Name
- 3,5-Dichlorobenzyl bromide
- Synonyms
- 105218;-3,5-dichlorobenzene;3,5-Dichlorobenzyl bromide;alpha-Bromo-3,5-dichlorotoluene;1-(bromomethyl)-3,5-dichlorobenzene;5-(Bromomethyl)-1,3-dichlorobenzene;Benzene, 1-(bromomethyl)-3,5-dichloro-
- CBNumber
- CB21140873
- Molecular Formula
- C7H5BrCl2
- Formula Weight
- 239.92
- MOL File
- 7778-01-0.mol
3,5-Dichlorobenzyl bromide Property
- Boiling point:
- 146-150 °C(Press: 18 Torr)
- Density
- 1.679±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C7H5BrCl2/c8-4-5-1-6(9)3-7(10)2-5/h1-3H,4H2
- InChIKey
- CTJIGYSODYOMGI-UHFFFAOYSA-N
- SMILES
- C1(CBr)=CC(Cl)=CC(Cl)=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H311Toxic in contact with skin
H314Causes severe skin burns and eye damage
H331Toxic if inhaled
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P311Call a POISON CENTER or doctor/physician.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P361Remove/Take off immediately all contaminated clothing.
P363Wash contaminated clothing before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- D6130
- Product name
- 1-(Bromomethyl)-3,5-dichlorobenzene
- Purity
- min. 98.0 %
- Packaging
- 1G
- Price
- $120
- Updated
- 2025/07/31
- Product number
- 5076AQ
- Product name
- 1-(bromomethyl)-3,5-dichlorobenzene
- Packaging
- 5g
- Price
- $212
- Updated
- 2021/12/16
- Product number
- 5076AQ
- Product name
- 1-(bromomethyl)-3,5-dichlorobenzene
- Packaging
- 10g
- Price
- $364.4
- Updated
- 2021/12/16
- Product number
- 131703
- Product name
- 1-(Bromomethyl)-3,5-dichlorobenzene
- Purity
- 97%
- Packaging
- 1g
- Price
- $478
- Updated
- 2021/12/16
- Product number
- HCH0063474
- Product name
- 1-(BROMOMETHYL)-3,5-DICHLOROBENZENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.5
- Updated
- 2021/12/16
3,5-Dichlorobenzyl bromide Chemical Properties,Usage,Production
Synthesis
60211-57-6
7778-01-0
General procedure: A solution of carbon tetrachloride (50 mL) of bromine (3.17 mL, 61 mmol) was slowly added dropwise to a solution of carbon tetrachloride (250 mL) of triphenylphosphine (16.13 g, 61 mmol) and mixed well with stirring. Subsequently, a solution of carbon tetrachloride (50 mL) of 3,5-dichlorobenzyl alcohol (10.0 g, 56 mmol) was added and the reaction mixture was heated to reflux and maintained for 45 minutes. Upon completion of the reaction, hexane was added for dilution. The mixture was filtered through a silica gel column and washed well with hexane. The filtrate was collected and the solvent was removed by concentration under reduced pressure to afford 3,5-dichlorobenzyl bromide (12.79 g, 95% yield). The product was characterized by 1H-NMR (400 MHz, CDCl3): δ= 4.37 (s, 2H), 7.24-7.28 (m, 3H).
References
[1] Patent: WO2006/120544, 2006, A1. Location in patent: Page/Page column 50
[2] Patent: WO2006/107923, 2006, A1. Location in patent: Page/Page column 70-71
[3] Bioorganic and Medicinal Chemistry Letters, 2000, vol. 10, # 8, p. 821 - 826
[4] Archiv der Pharmazie, 2005, vol. 338, # 7, p. 299 - 304
[5] Patent: WO2006/30984, 2006, A1. Location in patent: Page/Page column 63; 134
3,5-Dichlorobenzyl bromide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-Dichlorobenzyl bromide manufacturers
- Product
- 3,5-Dichlorobenzyl bromide 7778-01-0
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2024-08-05
- Product
- 3,5-Dichlorobenzyl bromide 7778-01-0
- Price
- US $101.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-28